Method for recovering valuable metals by electrolysis of high bismuth crude lead
A valuable metal, electrolytic recovery technology, applied in the direction of photography technology, instruments, photography auxiliary technology, etc., can solve the problem of no reported processing method, and achieve the effect of broadening the adaptability of raw materials, excellent recovery rate index, and high efficiency
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Embodiment 1
[0019] A method for recovering valuable metals by electrolysis of high bismuth crude lead: has the following steps:
[0020] 1. Mix and match high-bismuth crude lead containing 26.38% bismuth with crude lead containing less than 1.0% bismuth, and produce an anode plate after preliminary refining by fire method. The composition is as follows: Pb 86.22%, Bi 8.53%, Cu 0.09 %, Sb 2.51%, As 0.15%, Ag0.76%;
[0021] 2. Put the above-mentioned anode plate into the electrolytic cell for electrolytic refining. The process conditions are: current density 120 A / m 2 , cell voltage 0.40V, electrolyte circulation speed 26 l / min, electrolyte temperature 33°C, electrolyte solution containing lead ions 70g / l, total acid 160g / l, free acid 80g / l;
[0022] 3. After 24 hours of electrolytic refining, the anode plate in the electrolytic tank is lifted out and sent to the anode scrap washing machine for mechanical cleaning, and then hoisted into a special tank for manual cleaning with high-pressure...
Embodiment 2
[0026] A method for recovering valuable metals by electrolysis of high bismuth crude lead: has the following steps:
[0027] 1. Reasonably mix crude lead, and properly control the composition of the anode plate; that is, mix and match high-bismuth crude lead containing 35% bismuth with crude lead containing 0.2% bismuth, and then add 5% lead scum or lead dioxide ash by total weight , the anode plate is produced after preliminary refining by fire method, and its composition is as follows: Pb 88.31%, Bi 8.41%, Cu 0.10%, Sb 2.32%, As 0.19%, Ag 0.67%;
[0028] 2. Put the above-mentioned anode plate into the electrolytic cell for electrolytic refining, replenish lead ions in time to ensure the composition of the electrolyte; the process conditions are: current density 110 A / m 2 , cell voltage 0.50V, electrolyte circulation speed 20 l / min, electrolyte temperature 35°C, electrolyte solution containing lead ions 75 g / l, total acid 155 g / l, free acid 78 g / l;
[0029] 3. After 24 hours...
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