Black tomato glycerol triacetate extract and application thereof in cigarettes
A technology of tomato triacetin and triacetin, which is applied in application, tobacco, food science and other directions, can solve the problems of difficulty in cigarettes, increased production cost, limited solubility of additives, complicated preparation process, etc., and achieves rich natural tobacco fragrance. , the effect of strong operability and standardization, and simple production process
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Embodiment 1
[0021] Fresh black tomato stalks are removed and cleaned, drained, freeze-dried after beating, and the powder obtained after grinding is passed through a 60-mesh sieve, and 300g of black tomato freeze-dried powder is weighed and placed in a round-bottomed flask, and the ratio of material to liquid is 1: Add glycerol triacetate at a ratio of 5 as the extractant, soak at room temperature for 3 hours, then carry out reflux extraction at 60°C for 7 hours, and after cooling to room temperature, extract the black tomato after reflux extraction and glyceryl triacetate were placed in an ultrasonic extraction device (400W, 40kHZ), extracted for 30 minutes, and the filter residue was removed by filtration to obtain a clear solution, which was the desired black tomato triacetin extract.
[0022] Using triacetin as solvent, black tomato triacetin extract is prepared into a solution with a concentration of 3%, and evenly sprayed on the filter rod tow according to the weight ratio of 7% of t...
Embodiment 2
[0024] Fresh black tomato stalks are removed and cleaned, drained, freeze-dried after beating, and the powder gained from grinding is passed through a 40-mesh sieve, and 500g of black tomato freeze-dried powder is weighed and placed in a round-bottomed flask, according to the ratio of material to liquid: 1: Add glycerol triacetate at a ratio of 7 as the extractant, soak at room temperature for 5 hours, and then carry out reflux extraction at 80°C for 6 hours. After cooling to room temperature, the black tomato after reflux extraction and glyceryl triacetate are placed in an ultrasonic extraction device (600W, 40kHZ), extracted for 50 minutes, filtered to remove the filter residue to obtain a clear solution, and the desired black tomato triacetin extract can be obtained.
[0025] Using triacetin as solvent, black tomato triacetin extract is formulated into a solution with a concentration of 3%, and evenly sprayed on the filter rod tow according to the weight ratio of 7.5% of the...
Embodiment 3
[0027] Fresh black tomato stalks are removed and cleaned, drained, and then freeze-dried after beating. The powder obtained after grinding is passed through a 60-mesh sieve, and 400g of black tomato freeze-dried powder is weighed and placed in a round-bottomed flask. The ratio of material to liquid is 1: Add glycerol triacetate at a ratio of 10 as the extractant, soak at room temperature for 5 hours, then carry out reflux extraction at 60°C for 6 hours, and after cooling to room temperature, extract the black tomato after reflux extraction and glyceryl triacetate are placed in an ultrasonic extraction device (400W, 40kHZ), extracted for 20 minutes, filtered to remove the filter residue to obtain a clear solution, and the desired black tomato triacetin extract can be obtained.
[0028] Using triacetin as a solvent, black tomato triacetin extract was formulated into a solution with a concentration of 4%, and evenly sprayed on the filter rod tow in a proportion of 7% by weight of ...
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