Direct coal liquefaction process
A direct coal liquefaction technology, applied in the preparation of liquid hydrocarbon mixtures, petroleum industry, etc., can solve the problems of low solid content and liquid content, increase in coal residence time liquefaction reactor volume, high gas content, etc. The effect of reducing complexity and capital costs
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[0043]The process of the invention was carried out in the same 0.1 t / d pilot plant as used in the experiments described by Wasaka. The pilot plant was tuned for slurry mixing tank, pumps, slurry reactor, microcatalyst (molybdenum) addition and 600-700°F + recirculation. Compared with Wasaka's pilot plant operation, the slurry feed flow rate increased to 10-12kg / h, and the gas flow rate decreased by 2-4 times. During the run of the pilot plant, the reactor experienced no solids buildup or reactor deposits. The coal used in this example was in figure 1 The plot for is represented as a square symbol, and is thus consistent with the overall trend of H / C relative to inertinite content.
[0044] The oil yield at a non-donor 650°F+ (343°C) recycle stream to coal ratio of 1.5 / 1 was 44.6 wt% (on a MAF basis). When at 0.73Nm 3 Low H / kg slurry 2 The C5+ / 371°C (C5 / 650°F) yield increased to 66.4 wt% at the feed flow rate of 650°F+ when the stream ratio was increased to 3 / 1. This is ...
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