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Passive sampling device for atmospheric organic pollutant

A passive sampling device and organic pollutant technology, applied in the direction of sampling device, test sample preparation, etc., can solve the problems of low-density polyethylene film is easy to break, the wind speed sampling results are greatly affected, and the sampling rate is limited. Achieve the effect of simple sample processing procedure, fast sampling speed and increased contact area

Inactive Publication Date: 2015-06-10
浙江中一检测研究院股份有限公司
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AI Technical Summary

Problems solved by technology

[0004] CN201210172065.5 discloses a passive sampling device for persistent organic pollutants in the atmosphere. The method uses alkylated diatomite coated with silicone oil as the sampling medium, but there is only one layer of low-density polyethylene film between the sampling port and the atmosphere. , the wind speed has a great influence on the sampling results, and the low-density polyethylene film is easy to break, and it is difficult to operate in heavy rain and windy weather
CN201210474571.X discloses a passive sampling device for multi-component atmospheric organic pollutants, which supports and protects the sampling sieve drum through the stacking of multi-layer baffles, but the higher wind speed will also have a greater impact on the sampling results, and due to multiple Due to the weight factor of the baffle itself, the size of the entire sampling device should not be too large, and the sampling rate is also limited.
CN200910077064.0 discloses a passive sampling device for persistent organic pollutants. The method adopts the design of an inner cover and an outer cover for sampling, and two collection materials are respectively placed on the upper and lower sides of the inner cover to realize the simultaneous collection of gaseous pollutants and particulate pollutants. CN201310325898.5 discloses a passive sampling device for persistent organic pollutants, the contact area between the gaseous pollutants and the sampling medium is only the upper bottom surface of the cylindrical sampling device, the equivalent sampling volume is small, and the sampling rate is limited

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  • Passive sampling device for atmospheric organic pollutant
  • Passive sampling device for atmospheric organic pollutant
  • Passive sampling device for atmospheric organic pollutant

Examples

Experimental program
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Effect test

Embodiment

[0024] Example, the collection and measurement of PCBs in the atmosphere in an industrial park in a certain city

[0025] (1) Put XAD resin (a sampling material) into a low-density polyethylene film bag, seal it with a heat sealer and spread it on a clean table to form a uniform layer, and place it in the interlayer of the sampling material holder;

[0026] (2) At the sampling site, arrange 4 sampling devices about 150cm away from the ground to collect atmospheric samples;

[0027] (3) When the sampling time reaches 2, 4, 6, or 8 weeks, the sampling device shall be recovered, and the collected samples shall be stored at -20°C and brought back to the laboratory for analysis;

[0028] (4) The sample was extracted with a fast solvent extraction instrument ASE, the extraction solvent was acetone: methylene chloride 1:1, the temperature was 100°C, the pressure was 1650 psi, the static extraction time was 6 minutes, and the number of cyclic extractions was 3 times. The nitrogen purge volume...

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Abstract

The invention relates to a passive sampling device for atmospheric organic pollutant and belongs to the field of atmosphere environment monitoring. The passive sampling device for the atmospheric organic pollutant is aimed to provide a passive sampler featured with fast sampling speed rate, and easiness and convenience in sample processing. According to the technical scheme, the sampling device comprises a sampling material holding bracket, a semi-permeable membrane and sampling material; the sampling material holding bracket is a hollow column body, and a connecting device is arranged at each lateral surface of the hollow column body to form an interlayer between the two lateral surfaces of the hollow column body; the semi-permeable membrane is placed in the interlayer of the sampling material holding bracket; the sampling material is placed in the semi-permeable membrane, and a semi-permeable membrane is arranged between the sampling material and the sampling material holding bracket.

Description

Technical field [0001] The invention relates to a passive sampling device for atmospheric organic pollutants, belonging to the field of atmospheric environment monitoring. Background technique [0002] With the rapid development of urbanization and industrialization in my country in recent years, the problem of urban air environmental pollution has become more and more serious, bringing many health and safety hazards and threats to urban residents. With the continuous development of many advanced analysis methods, the level of analysis and testing of environmental samples has been greatly improved. However, the collection of environmental atmospheric samples is still limited by many conditions. Currently, the commonly used atmospheric active (such as large-volume air samplers) sampling equipment is large in size and needs to be driven by electric power, making it difficult to conduct large-scale sampling in the field. In order to solve this problem, some scholars put forward the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/22G01N1/34
Inventor 何莲李怀瑞张皓朱华斌王炎震陈钊增
Owner 浙江中一检测研究院股份有限公司
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