Passive sampling device for atmospheric organic pollutant
A passive sampling device and organic pollutant technology, applied in the direction of sampling device, test sample preparation, etc., can solve the problems of low-density polyethylene film is easy to break, the wind speed sampling results are greatly affected, and the sampling rate is limited. Achieve the effect of simple sample processing procedure, fast sampling speed and increased contact area
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[0024] Example, the collection and measurement of PCBs in the atmosphere in an industrial park in a certain city
[0025] (1) Put XAD resin (a sampling material) into a low-density polyethylene film bag, seal it with a heat sealer and spread it on a clean table to form a uniform layer, and place it in the interlayer of the sampling material holder;
[0026] (2) At the sampling site, arrange 4 sampling devices about 150cm away from the ground to collect atmospheric samples;
[0027] (3) When the sampling time reaches 2, 4, 6, or 8 weeks, the sampling device shall be recovered, and the collected samples shall be stored at -20°C and brought back to the laboratory for analysis;
[0028] (4) The sample was extracted with a fast solvent extraction instrument ASE, the extraction solvent was acetone: methylene chloride 1:1, the temperature was 100°C, the pressure was 1650 psi, the static extraction time was 6 minutes, and the number of cyclic extractions was 3 times. The nitrogen purge volume...
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