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Regular catalyst packing for reactive distillation column

A technology of reactive distillation column and catalytic packing, which is applied in the field of high-efficiency structured catalytic packing, can solve the problems of packing layer blockage, liquid channeling, and insufficient tightness, and achieve the goals of reducing equipment investment costs, increasing reaction conversion rate, and improving utilization rate Effect

Active Publication Date: 2015-05-06
FUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this kind of packing has the following disadvantages: (1) The particle size of catalyst particles and porous inert balls is generally small, which is easy to cause plugging of the packing layer in the tower; (2) When the metal box structure is placed in the tower, it is not tight enough, which is easy to cause Phenomena such as channel flow and short circuit of the liquid in the tower
Although this structure eliminates the problems of liquid channeling and short circuit, it has the disadvantages of large catalyst bed resistance and small processing capacity of catalytic distillation tower.

Method used

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  • Regular catalyst packing for reactive distillation column
  • Regular catalyst packing for reactive distillation column
  • Regular catalyst packing for reactive distillation column

Examples

Experimental program
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Effect test

Embodiment 1

[0026] Component A, which uses stainless steel orifice plate corrugated packing as structured catalytic packing, has a pore mesh of 80 mesh, and the inclination direction of the corrugation forms an included angle of 45° with the horizontal direction; component B uses polyester sewed catalyst cloth as the structured catalytic packing , and the cloth bags are sewed into cloth bags with a side-by-side width of 120mm at equal intervals, and glass microspheres are filled in the cloth bags as catalysts, and the filling height is 70% of the cloth bag height. The heights of the catalyst cloth bag and the stainless steel corrugated wire mesh are both 200mm, and the overall length is adjusted according to different positions of the structured catalytic packing. Each layer of structured catalytic packing has 10 pieces of stainless steel corrugated wire mesh and 10 pieces of catalyst cloth bag, 20 pieces in total. Place the stainless steel corrugated wire mesh and catalyst cloth bag alter...

Embodiment 2

[0028] Stainless steel corrugated wire mesh is used as component A of the structured catalytic packing, the mesh number of which is 30 mesh, and the inclined direction of the corrugation is at an angle of 45° to the horizontal direction; the component B made of polypropylene fiber as a catalyst cloth bag is used as the structured catalytic packing , and the cloth bags are sewed into cloth bags with a side-by-side width of 100mm at equal intervals, and then filled with resin as a catalyst in the cloth bag, and its filling height is 80% of the height of the cloth bag. The height of the stainless steel corrugated wire mesh and the catalyst cloth bag is 500mm, and the overall length is adjusted according to the different positions of the structured catalytic packing. Each layer of structured catalytic packing has 15 pieces of stainless steel corrugated wire mesh and 15 pieces of catalyst cloth bags, 30 pieces in total. Place the stainless steel corrugated wire mesh and catalyst clo...

Embodiment 3

[0030] Stainless steel corrugated wire mesh packing is used as component A of the structured catalytic packing, the mesh number of which is 50 mesh, and the inclined direction of the corrugation is at an angle of 60° to the horizontal direction; the catalyst cloth bag sewn with nylon cloth is used as the structured catalytic packing Component B, and the cloth bags are sewn into cloth bags with a side-by-side width of 80 mm, and then filled with molecular sieves as catalysts, and the filling height is 90% of the cloth bag height. The heights of the catalyst cloth bag and the stainless steel corrugated wire mesh are both 300mm, and the overall length is adjusted according to different positions of the structured catalytic packing. There are 10 pieces of stainless steel corrugated wire mesh and 10 pieces of catalyst cloth bag in each layer of structured catalytic packing, 20 pieces in total. The stainless steel corrugated wire mesh and catalyst cloth bag are placed alternately to ...

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Abstract

The invention discloses a regular catalyst packing for a reactive distillation column. The regular catalyst packing is composed of a component (A) and a component (B), wherein the component (A) and the component (B) are arrayed alternatively and then banded by a banding piece; the component (A) is composed of a plurality of corrugated packing pieces with meshed structure or pore canal structure; the component (B) is a cloth bag evenly sewed and filled with particle solid catalysts; in each regular catalyst packing, the component (A) and the component (B) are arranged alternatively; the corrugated inclination direction of each two adjacent corrugated packing pieces are reverse. By utilizing the corrugated packing pieces, the whole catalyst packing layer can have enough passage, the gas and liquid can be distributed better in the column, and the dead area and uneven flow of liquid are avoided; by utilizing the catalyst cloth bag, the use amount of catalyst can be reduced; with the combination of the corrugated packing pieces and the catalyst cloth bag, the contact time of the reactant and catalyst is longer, so the reactive distillation process is performed efficiently. Meanwhile, the regular catalyst packing is easy to manufacture and convenient to assemble and disassemble, and the requirements of industrial production can be met.

Description

technical field [0001] The invention belongs to the technical field of reactive distillation, and in particular relates to a high-efficiency structured catalytic packing suitable for reactive distillation towers. Background technique [0002] Reactive distillation is a process of reaction and separation at the same time, so the packing in the reactive distillation column needs to have two functions at the same time: catalytic function and gas-liquid mass transfer function, so as to separate the product during the reaction and promote the reaction to continue to increase conversions. Among them, the packing structure in the tower has a great influence on the efficiency of the reactive distillation process. The packing used in industry is mainly divided into random packing and structured packing. Random packing is placed directly in the tower, and its pressure drop is relatively large. The layer is easy to block; while the structured packing requires a balance between the cat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/32
CPCB01J19/32B01J2219/30408B01J2219/30475
Inventor 李玲张小武王清莲王红星叶长燊杨臣黄智贤邱挺
Owner FUZHOU UNIV
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