Anti-radiation film type building energy-saving material based on silica acrylic acid fused ceramic composite material and preparation method of anti-radiation film type building energy-saving material
A technology of ceramic composite materials and silicon acrylic acid, applied in the direction of coating, etc., can solve the problems of shortening the service life of buildings, falling off of surface decoration materials, cracking of building walls, etc., and achieve outstanding heat resistance, long-lasting heat insulation effect, and long-lasting color Effect
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Embodiment 1
[0032] Denatured Silicone Acrylic Emulsion Formulation:
[0033] Methyl methacrylate 32%
[0034] Styrene 3%
[0035] Butyl Acrylate 45%
[0036] Acrylic 2%
[0038] Octamethylcyclotetrasiloxane 8%
[0039] Ammonium persulfate 0.35%
[0040] Sodium dodecyl sulfonate 0.05%
[0041]Sufficient deionized water.
[0042] The preparation method is as follows:
[0043] 1) Preparation of denatured silicone acrylic acid emulsion: Add distilled water and polyvinyl alcohol to a four-necked flask equipped with a condenser, agitator, thermometer, and dropping funnel to raise the temperature to 90°C and keep it warm for 15 minutes, then cool the system down to 80°C. Add emulsifier, part of initiator, part of acrylic monomer, stir at constant temperature for 1 hour, then add the remaining mixed solution of acrylic monomer and initiator dropwise at a constant speed, when there is 10% of acrylic monomer left, put it in the dropping funnel Add organosilicon...
Embodiment 2
[0049] Denatured Silicone Acrylic Emulsion Formulation:
[0050] Methyl methacrylate 33%
[0051] Styrene 4%
[0052] Butyl Acrylate 44%
[0053] Acrylic 2%
[0054] Silicone monomer 4%
[0055] Octamethylcyclotetrasiloxane 10%
[0056] Ammonium persulfate 0.35%
[0057] Sodium dodecyl sulfonate 0.086%
[0058] Sufficient deionized water.
[0059] The preparation method is as follows:
[0060] 1) Preparation of denatured silicone acrylic acid emulsion: Add distilled water and polyvinyl alcohol to a four-necked flask equipped with a condenser, agitator, thermometer, and dropping funnel to raise the temperature to 90°C and keep it warm for 15 minutes, then cool the system down to 80°C. Add emulsifier, part of initiator, part of acrylic monomer, stir at constant temperature for 1 hour, then add the remaining mixed solution of acrylic monomer and initiator dropwise at a constant speed, when there is 10% of acrylic monomer left, put it in the dropping funnel Add organosili...
Embodiment 3
[0066] Denatured Silicone Acrylic Emulsion Formulation:
[0067] Methyl methacrylate 35%
[0068] Styrene 5%
[0069] Butyl Acrylate 43%
[0070] Acrylic 2%
[0071] Silicone monomer 3%
[0072] Octamethylcyclotetrasiloxane 8%
[0073] Ammonium persulfate 0.35%
[0074] Sodium dodecyl sulfonate 0.095%
[0075] Sufficient deionized water.
[0076] The preparation method is as follows:
[0077] 1) Preparation of denatured silicone acrylic acid emulsion: Add distilled water and polyvinyl alcohol to a four-necked flask equipped with a condenser, agitator, thermometer, and dropping funnel to raise the temperature to 90°C and keep it warm for 15 minutes, then cool the system down to 80°C. Add emulsifier, part of initiator, part of acrylic monomer, stir at constant temperature for 1 hour, then add the remaining mixed solution of acrylic monomer and initiator dropwise at a constant speed, when there is 10% of acrylic monomer left, put it in the dropping funnel Add organosilic...
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