A preparation method of a composite adsorption material that simultaneously adsorbs heavy metal ions and volatile organic compounds in waste gas
A technology of composite adsorption materials and volatile organic compounds, which is applied in separation methods, chemical instruments and methods, and separation of dispersed particles. It can solve the problems of no adsorbent, which affects the cost and effect of waste gas treatment, and achieves short adsorption time and high adsorption performance. The effect of improvement and stable performance
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Embodiment 1
[0023] 1) Pretreatment of carbon nanotubes: Put carbon nanotubes into a mixed solution of concentrated nitric acid and hydrofluoric acid, soak them under high pressure in an argon environment, maintain them at 120°C for 10 hours, cool them to room temperature, and then take out the carbon nanotubes. The nanotubes are washed and filtered with deionized water, and set aside;
[0024] 2) Preparation of calcium chloride: hydrochloric acid enters the reaction tank, and limestone is lifted into the reaction tank through a bucket elevator. After the reaction, the gas is washed with water in the tail gas scrubber and alkali washed in the tail gas scrubber, and the gas reaches the standard and is discharged by the induced draft fan. After the pH value of the liquid reaches 5, it enters the neutralization tank directly through the bypass pipe, and after adding lime milk to react, it is poured into the clarification tank through the neutralization pump, and the clarified liquid overflows ...
Embodiment 2
[0033] 1) Pretreatment of carbon nanotubes: Put carbon nanotubes into a mixed solution of concentrated nitric acid and hydrofluoric acid, soak them under high pressure in an argon environment, maintain at 150°C for 15 hours, cool to room temperature, and then take out the carbon nanotubes. The nanotubes are washed and filtered with deionized water, and set aside;
[0034] 2) Preparation of calcium chloride: hydrochloric acid enters the reaction tank, and limestone is lifted into the reaction tank through a bucket elevator. After the reaction, the gas is washed with water in the tail gas scrubber and alkali washed in the tail gas scrubber, and the gas reaches the standard and is discharged by the induced draft fan. After the pH value of the liquid reaches 7, it enters the neutralization tank directly through the bypass pipe, and after adding lime milk to react, it is poured into the clarification tank through the neutralization pump, and the clarified liquid overflows into the c...
Embodiment 3
[0043] 1) Pretreatment of carbon nanotubes: Put carbon nanotubes into a mixed solution of concentrated nitric acid and hydrofluoric acid, soak them under high pressure in an argon environment, maintain them at 130°C for 18 hours, cool them to room temperature, and then take out the carbon nanotubes. The nanotubes are washed and filtered with deionized water, and set aside;
[0044] 2) Preparation of calcium chloride: hydrochloric acid enters the reaction tank, and limestone is lifted into the reaction tank through a bucket elevator. After the reaction, the gas is washed with water in the tail gas scrubber and alkali washed in the tail gas scrubber, and the gas reaches the standard and is discharged by the induced draft fan. After the pH value of the liquid reaches 6, it enters the neutralization tank directly through the bypass pipe, and after adding lime milk to react, it is poured into the clarification tank through the neutralization pump, and the clarified liquid overflows ...
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