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Phosphorus-free textile scouring agent

A scouring agent and textile technology, which is applied in the field of saponin-free textile scouring agent, can solve the problems of poor wool effect and whiteness, low permeability and wettability, etc., and achieve good hair effect, whiteness, and penetration The effect of improving performance and wetting and dispersing properties

Active Publication Date: 2014-10-15
SHANGHAI DUOLUN CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] One of the technical problems to be solved in the present invention is that the existing saponin-containing non-phosphorous textile scouring agent has low permeability and wettability, thus causing poor wool effect and whiteness. A new non-phosphorous textile scouring agent is provided, It has the advantages of strong permeability and wettability, good capillary effect and whiteness

Method used

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  • Phosphorus-free textile scouring agent
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  • Phosphorus-free textile scouring agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] 1. Synthesis of Fatty Alcohol Ether

[0064] Into a dry 2 L reaction kettle with stirring, electric heating mantle and internal water cooling coil was charged 2 moles of tetradecyl alcohol and potassium hydroxide. Seal the reaction kettle, replace the air in the reaction kettle with nitrogen for three times, start stirring, heat up to 80°C and carry out vacuum treatment under the gauge pressure of -0.07MPa for 60 minutes, then raise the temperature to 120°C and maintain this temperature, and pass through ethylene oxide 18 moles of alkylene oxide mixture (10 moles of ethylene oxide, 8 moles of propylene oxide), keep the gauge pressure of the reactor at 0.15MPa by controlling the feed rate of the ethylene oxide mixture, and add the epoxy After the mixture of ethylene oxide and propylene oxide, mature at 120°C for 1 hour, then add 6 moles of ethylene oxide, keep the gauge pressure of the reactor at 0.15Mpa by controlling the speed of adding ethylene oxide, mature at 120°C ...

Embodiment 2

[0071] 1. Synthesis of Fatty Alcohol Ether

[0072] Into a dry 2 L reaction kettle with stirring, electric heating mantle and internal water cooling coil was charged 2 moles of tetradecyl alcohol and potassium hydroxide. Seal the reaction kettle, replace the air in the reaction kettle with nitrogen for three times, start stirring, heat up to 80°C and carry out vacuum treatment under the gauge pressure of -0.07MPa for 60 minutes, then raise the temperature to 120°C and maintain this temperature, and pass through ethylene oxide 10 moles of alkanes, the gauge pressure of the reactor is kept at 0.15 MPa by controlling the feeding speed of ethylene oxide, after the addition of ethylene oxide, it is matured at 120°C for 1 hour, and then 8 moles of propylene oxide are fed in, and the pressure is controlled by controlling the loop The feeding speed of propylene oxide keeps the gauge pressure of the reactor at 0.15MPa. After adding propylene oxide, it is aged at 120°C for 1 hour, and t...

Embodiment 3

[0079] 1. Synthesis of Fatty Alcohol Ether

[0080] Into a dry 2 L reaction kettle with stirring, electric heating mantle and internal water cooling coil was charged 2 moles of tetradecyl alcohol and potassium hydroxide. Seal the reaction kettle, replace the air in the reaction kettle with nitrogen for three times, start stirring, heat up to 80°C and carry out vacuum treatment at a gauge pressure of -0.07MPa for 60 minutes, then raise the temperature to 120°C and maintain this temperature, and pass in propylene oxide 8 moles, keep the gauge pressure of the reactor at 0.15MPa by controlling the feed rate of propylene oxide, after adding propylene oxide, mature at 120°C for 1 hour, then feed 16 moles of ethylene oxide, The feed rate of alkane keeps the gauge pressure of the reactor at 0.15MPa. After adding ethylene oxide, mature at 120°C for 1 hour, cool down to 70°C, neutralize with acetic acid, and then carry out vacuum dehydration at a gauge pressure of -0.07MPa The fatty al...

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Abstract

The invention relates to a phosphorus-free textile scouring agent, and solves the problem that the conventional phosphorus-free textile scouring agent has poor permeability and wettability. The novel phosphorus-free textile scouring agent comprises components in parts by weight as follows: 5-20 parts of saponin, 5-20 parts of fatty alcohol ether and 100 parts of an anionic surfactant, wherein the fatty alcohol ether has the general formula shown as the following formula (I): R-O-[(PO)n / (EO)m]-(EO)t-H, wherein R is C8-C18 alkyl; [(PO)n / (EO)m] is a copolymerized chain segment formed by PO and EO, the number n of PO units in the copolymerized chain segment ranges from 2 to 5, and the number m of EO units in the copolymerized chain segment ranges from 2 to 8, and the number t of EO structural units at the tail end of the molecule in the general molecular formula ranges from 2 to 5. With adoption of the technical scheme, the technical problem is better solved, and the phosphorus-free textile scouring agent can be applied to dyeing pretreatment processes for various textile fabric such as cotton, wool, linen, silk, synthetic fiber and the like.

Description

technical field [0001] The invention relates to a non-phosphorous textile scouring agent, especially a non-phosphorous textile scouring agent comprising saponin. Background technique [0002] The scouring process is a complex chemical and physical chemical process of textiles at a certain temperature with alkali and scouring agents, which includes penetration, cleaning, puffing, emulsification, saponification, dispersion, chelation and decolorization, among which penetration and purification Washing is a relatively important function. The first step in the scouring process is that under the action of surfactants, the scouring liquid penetrates into the fiber to make the fibers and impurities expand; the second step is the cleaning function, that is, after the fiber is fully wetted, its Impurities are removed by heat and chemical soaping, emulsification, extraction, dispersion, etc. The role of the scouring agent is to help the lye penetrate into the fiber, promote the sapon...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/11D06M13/165D06M15/53
Inventor 李翔朱学文徐兴建舒建生林真意侯海育
Owner SHANGHAI DUOLUN CHEM
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