Application of hibiscus root extractive in cigarette tobacco
A technology of root extract and hollyhock, which is applied in the application field of humectant in cigarettes, can solve the problems that have not been seen in the application of hollyhock root extract, and achieve the effects of rich production raw materials, improved moisturizing performance, and reduced miscellaneous gas
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Embodiment 1
[0018] Take the dried hollyhock root, use a wood crusher to crush it into particles with a diameter less than 5 mm; add distilled water for extraction at 70°C for 3 hours, water: material (mass ratio) = 15:1; filter with a 400-mesh filter cloth Take out the extract, concentrate under reduced pressure to 1 / 5 of the original volume; add the same volume of Sevag reagent as the concentrated solution, fully shake for 30 min, let stand until the solution is separated, and remove the thick Sevag reagent and denatured protein in the lower layer. mixture; repeat the deproteinization operation 2 times. Concentrate the deproteinized supernatant to 1 / 3 of the original volume, and then add it to 95% ethanol, so that the volume fraction of ethanol in the system reaches 80%; stand at 2-6°C for 12 hours, and depressurize The precipitate is separated by suction filtration, the precipitate is washed with absolute ethanol and acetone in turn, and freeze-dried to obtain the marshmallow root extra...
Embodiment 2
[0024] Take the dried hollyhock root, use a wood chip machine to crush it into thin slices with a thickness of about 1 mm; add water for extraction at 80°C for 2 hours, water: material (mass ratio) = 10:1, extract twice; combine the two dipping Extract the solution, concentrate it under reduced pressure to 1 / 10 of the original volume; add Sevag reagent 0.8 times the volume of the concentrated solution, shake fully for 30 min, let stand until the solution is separated, remove the mixture of the lower layer of thick Sevag reagent and denatured protein, This deproteinization operation was repeated 3 times. Concentrate the deproteinized supernatant to 1 / 5 of the original volume, and then add it to 95% ethanol, so that the volume fraction of ethanol in the system reaches 85%; stand at 2-6°C for 6 hours, and depressurize The precipitate is separated by suction filtration, and the obtained precipitate is washed with absolute ethanol and acetone in sequence, and freeze-dried to obtain...
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