Refined method for crude sulfate turpentine
A technology of sulfate turpentine and refining method, which is applied to chemical instruments and methods, purification/separation of hydrocarbons, hydrocarbons, etc., can solve problems such as difficulty in obtaining ultra-low thiopinene products, and achieves high industrial reliability and method. Simple and effective results
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Embodiment 1
[0036] The mass composition of crude sulfate turpentine raw material is: pinene (α-pinene and β-pinene) 82%, total sulfur 1023ppm, water 0.3%, solid impurities 0.21%, and the rest are other terpenoid components.
[0037] (1) The crude sulfate turpentine raw material is preheated at 55°C by heat exchanger E-1 at a rate of 12kg / h, and then enters flash tower T-1 from pipeline 1 for flash separation treatment. The temperature in the flash tower is 102°C, the temperature of the reboiler in the packing separation section is 104°C. Light sulfur components such as sulfides and mercaptans with a boiling point lower than α-pinene flowing out from the top of the flash tower are output to the alkali neutralization absorption system R-2 through pipeline 2, and are neutralized by existing methods Direct discharge; while the initial desulfurization material (with a sulfur content of 35.4ppm) flowing out from the bottom of the flash tower is output to the vacuum rectification tower T-2 throu...
Embodiment 2
[0042] The mass composition of crude sulfate turpentine raw material is: pinene (α-pinene and β-pinene) 88%, total sulfur 897ppm, moisture 0.35%, solid impurities 0.33%, and the rest are other terpenoid components.
[0043] (1) The crude sulfate turpentine raw material is preheated to 60°C through the heat exchanger E-1 at a rate of 14kg / h, and then enters the flash tower T-1 from the pipeline 1 for flash separation treatment. The temperature in the flash tower is 101°C, and the reboiler temperature in the packing separation section is 103°C. Light sulfur components such as sulfides and mercaptans with a boiling point lower than α-pinene flowing out from the top of the flash tower are output to the alkali neutralization absorption system R-2 through pipeline 2, and are neutralized by existing methods Direct discharge; while the initial desulfurized material (with a sulfur content of 32.3ppm) flowing out from the bottom of the flash tower is output to the vacuum rectification t...
Embodiment 3
[0048] The mass composition of crude sulfate turpentine raw material is: pinene (α-pinene and β-pinene) 81%, total sulfur 623ppm, moisture 0.31%, solid impurities 0.19%, and the rest are other terpenoid components.
[0049] (1) The crude sulfate turpentine raw material is preheated to 66°C through the heat exchanger E-1 at a rate of 10kg / h, and then enters the flash tower T-1 from the pipeline 1 for flash separation treatment. The temperature in the flash tower is 105°C, and the temperature of the reboiler in the packing separation section is 107°C. Light sulfur components such as sulfides and mercaptans with a boiling point lower than α-pinene flowing out from the top of the flash tower are output to the alkali neutralization absorption system R-2 through pipeline 2, and are neutralized by existing methods Direct discharge; while the initial desulfurization material (with a sulfur content of 33.7ppm) flowing out from the bottom of the flash tower is output to the vacuum recti...
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