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Technology for refining saccharose

A sucrose and process technology, applied in the production of sugar, sugar crystallization, juice extraction from sugar cane, etc., can solve the problems of wasting energy, uneconomical and reasonable, increasing production costs, etc., and achieves reduction of labor input, significant economic benefits, The effect of saving labor costs

Active Publication Date: 2014-04-16
JIANGSU JIUWU HITECH
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Problems solved by technology

The "two-step method" requires large investment, complicated process, and high production cost, so it is not suitable for promotion in China; the sucrose produced by the carbonic acid method is of good quality, but the process is complicated, the process is long, the investment is large, and the environmental pollution is serious; The sulfuric acid method is currently the main sugar production method in China because of its relatively mature technology and relatively small investment.
However, this process also has many disadvantages: first, the process uses lime precipitation to remove impurities, and after plate and frame press filtration, a large amount of residue will be produced, which will seriously pollute the environment; secondly, the decolorization of this process is to use sulfur Smoked method, there will be sulfur residue in the product, which is harmful to human health. With the further improvement of the country's food safety requirements, this method will be restricted in use; third, the lime used in this method needs to be calcined. On the one hand, it consumes Larger energy is accompanied by waste discharge, and at the same time, a process section is added, which increases production costs; fourth, the concentration process of this method uses a multi-effect evaporator, which has high energy consumption and high production costs; fifth. , the process is relatively complicated, there are many equipments, and the area is large, and the control process is complicated
This method has the following disadvantages: first, the plate and frame filter press is used, which is relatively traditional, low in automation, and labor-intensive equipment. The working environment of the equipment is harsh and the production efficiency is low; For ultrafiltration membranes, there is no microfiltration membrane pretreatment in front, and the sugar liquid contains more macromolecular substances such as colloids and starches, which will cause low membrane flux, easy clogging of membrane pores, difficult cleaning, and poor practical operability; and The temperature of this part of the process is above 40°C. The organic membrane is not resistant to high temperature, and the life of the membrane will be relatively short, which is uneconomical and reasonable. The ash content is high, the quality is low or unqualified; fourth, the traditional three-effect evaporator is used, which wastes a lot of energy. Compared with advanced technologies such as MVR, the energy consumption is higher
Fifth, the relevant process parameters have not been optimized, resulting in waste of energy

Method used

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  • Technology for refining saccharose

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Effect test

Embodiment 1

[0046] Such as figure 1 Shown, the novel technique of sucrose refining of the present invention comprises the following steps:

[0047] A. Juicing: squeeze the sugarcane through a juice extractor to obtain sugarcane juice;

[0048] B, pretreatment: the sugarcane juice obtained in the step A is pretreated by a sieve to remove larger bagasse, and the aperture of the sieve is 100 orders;

[0049] C, microfiltration membrane filtration: the sugarcane juice collected in step B is microfiltered through a 50nm ceramic membrane, the temperature of the filtration is 20° C., and the filtration pressure is 0.5Mpa to obtain a sucrose juice clear liquid with a sucrose concentration of 12%;

[0050] D, pre-concentration: the sucrose juice obtained in step C is sent to the second-effect evaporator for evaporation and pre-concentration, and the sucrose concentration is concentrated to 40%;

[0051] E. Ion exchange decolorization: the concentrated sucrose juice obtained in step D is decolori...

Embodiment 2

[0063] Such as figure 1 As shown, the new process for refining sucrose of the present invention comprises the following steps: sugarcane juice is obtained after the sugarcane is squeezed, and the sugarcane juice is pretreated through a 200-mesh screen to remove larger bagasse to obtain sugarcane juice; the sugarcane juice is passed through a 200nm Ceramic membrane microfiltration, the filtration temperature is 80°C, and the filtration pressure is 0.1Mpa to obtain the sucrose juice serum with a concentration of 12.5%; the sugarcane juice serum enters the nanofiltration membrane device for concentration, and the nanofiltration membrane is made of ceramic material. The molecular weight is 100Da, the control pressure is 4.0MPa, the sugar juice concentration is 30%, and the salt removal rate is 53%. The concentrated sucrose juice enters the macroporous strong basic anion exchange resin for decolorization. The diameter-to-height ratio is 1 / 10, the flow rate is 2BV / h, and the tempera...

Embodiment 3

[0067] Such as figure 1 As shown, the new process for refining sucrose in the present invention comprises the following steps: pressing sugarcane through a juicer to obtain sugarcane juice; then pre-treating the sugarcane juice through a filter bag filter to remove larger bagasse, and then passing it through a 500nm Ceramic membrane microfiltration, the filtration temperature is 50°C, and the filtration pressure is 0.3Mpa to obtain sucrose juice clear liquid with a concentration of 11.5%; then the obtained sucrose juice is sent to an organic nanofiltration membrane concentration device, and the sucrose juice is obtained at a pressure of 4.0 Mpa, the nanofiltration membrane with a molecular weight of 100Da is pre-concentrated, so that the concentration of the sugar juice is concentrated to 30%, and 57% of the salt is removed. Then the obtained concentrated sucrose juice is decolorized with a macroporous strong basic anion exchange resin, the diameter-to-height ratio is 1 / 8, the...

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Abstract

The invention discloses a technology for refining saccharose. The technology comprises specific steps of juicing, pretreating, micro-filtering by a membrane, pre-concentrating, decoloring through ion exchange, desalting, evaporating and concentrating through MVR (mechanical vapor recompression), crystallizing, separating through centrifuging, and drying so as to obtain the saccharose crystal. The technology has the advantages that ceramic microfiltration substitutes for sedimentation by sheet frames and lime, so that the step of ultrafiltration is saved; due to concentration by the membrane, the evaporation capacity of evaporation and concentration equipment is reduced, the energy consumption is lowered, and part of inorganic salt is removed; the technology of decoloring and removing impurities through ion exchange substitutes for the technology of stoving, so that the problem of residual sulphur in the saccharose is solved, and the quality of the product is improved; the manner of ion exchange can effectively remove the salt in cane juice; energy consumption is effectively lowered due to the MVR; by adopting the membrane concentration and separation and ion exchange equipment, the floor space of the equipment is reduced, and investment of capital construction is lowered.

Description

technical field [0001] The invention relates to a sucrose refining process, in particular to a refining process. Background technique [0002] The so-called "one-step method" usually refers to the on-site processing of sugar materials (sugar cane, sugar beet) in the field sugar factory in the sugar production area to directly produce finished sugar, that is, "farmland sugar"; including: cultivated land white granulated sugar, cultivated land Brown sugar, cultivated brown sugar, etc. The sugar produced by the "one-step method" can be roughly divided into carbonation (clean process) sugar, sulfite process (clean process) sugar, lime process (clean process) sugar, etc. due to different processing and cleaning processes. [0003] All beet sugar factories in the world adopt the "one-step process" and adopt the carbonation method to clean the sugar beet land; with the improvement of beet quality and process technology, the quality of sugar beet land has reached the top grade, and...

Claims

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Application Information

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IPC IPC(8): C13B10/02C13B20/14C13B20/16C13B30/02
Inventor 彭文博凌国庆张宇江健张宏
Owner JIANGSU JIUWU HITECH
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