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White granulated sugar refining method

A refining method, white sugar technology, applied in the field of white sugar refining, can solve the problems of high production cost, harmful to human health, increased production cost, etc., achieve the effect of solving sulfur residue, avoiding pollution, and reducing production cost

Inactive Publication Date: 2020-06-05
彭冬元
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this process also has many disadvantages: first, the process uses lime precipitation to remove impurities, and after plate and frame press filtration, a large amount of residue will be produced, which will seriously pollute the environment; secondly, the decolorization of this process is to use sulfur Smoked method, there will be sulfur residue in the product, which is harmful to human health. With the further improvement of the country's food safety requirements, this method will be restricted in use; third, the lime used in this method needs to be calcined. On the one hand, it consumes Larger energy is accompanied by waste discharge, and at the same time, a process section is added, which increases production costs; fourth, the concentration process of this method uses a multi-effect evaporator, which has high energy consumption and high production costs; fifth. , the process is relatively complicated, there are many equipments, and the area is large, and the control process is complicated

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A. Juicing: squeeze the sugarcane through a juice extractor to obtain sugarcane juice;

[0033] B, pretreatment: the sugarcane juice obtained in the step A is pretreated by a sieve to remove larger bagasse, and the aperture of the sieve is 100 orders;

[0034] C, microfiltration membrane filtration: the sugarcane juice collected in step B is microfiltered through a 50nm ceramic membrane, the temperature of the filtration is 20°C, and the filtration pressure is 0.5Mpa to obtain a sucrose juice clear liquid with a sucrose concentration of 12%;

[0035] D, pre-concentration: the sucrose juice obtained in step C is sent to the second-effect evaporator for evaporation and pre-concentration, and the sucrose concentration is concentrated to 40%;

[0036] E. Ion exchange decolorization: the concentrated sucrose juice obtained in step D is decolorized with a macroporous strong basic anion exchange resin, the diameter-to-height ratio is 1 / 3, the flow rate is 10BV / h, and the tempe...

Embodiment 2

[0048] (1) Sugarcane juice is obtained after the sugarcane is squeezed, and the sugarcane juice is pretreated through a 200-mesh screen to remove larger bagasse to obtain sugarcane juice.

[0049] (2) The sugarcane juice is microfiltered through a 200nm ceramic membrane at a temperature of 80° C. and a filtration pressure of 0.1 Mpa to obtain a sucrose juice serum with a concentration of 12.5%.

[0050] (3) The sugarcane juice supernatant enters the nanofiltration membrane device for concentration. The material of the nanofiltration membrane is ceramic, the molecular weight cut-off is 100Da, the control pressure is 4.0MPa, the sugar juice concentration is 30%, and the salt removal rate is 53%.

[0051] (4) The concentrated sucrose juice enters the macroporous strong basic anion exchange resin for decolorization, the diameter-to-height ratio is 1 / 10, the flow rate is 2BV / h, and the temperature is 80°C. The chromaticity of the obtained sucrose solution is 250IU, and the average d...

Embodiment 3

[0057] (1) Squeeze the sugarcane through a juicer to obtain sugarcane juice; then pretreat the sugarcane juice through a filter bag filter to remove larger bagasse, and then pass it through a 500nm ceramic membrane microfiltration at a temperature of 50°C. The pressure is 0.3Mpa, and the sucrose juice serum is obtained with a concentration of 11.5%.

[0058] (2) then the sucrose juice obtained is sent into the organic nanofiltration membrane concentrating device, and the sucrose juice is initially pre-concentrated in the nanofiltration membrane with a molecular weight of 100Da at a pressure of 4.0Mpa, so that the concentration of the sugar juice is concentrated to 30%, and 57% of the salt was removed.

[0059] (3) decolorize the concentrated sucrose juice obtained with a macroporous strong basic anion exchange resin, the diameter-to-height ratio is 1 / 8, the flow rate is 4BV / h, and the temperature is 60°C. The sucrose solution chromaticity obtained is 460IU, the average decolo...

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Abstract

The invention discloses a white granulated sugar refining method which comprises the steps of cane sugar juicing, pretreatment, membrane microfiltration, pre-concentration, ion exchange decoloration,desalination, evaporation concentration, crystallization, centrifugal separation, drying and the like to obtain crystallized white granulated sugar. According to the method, ceramic microfiltration isused for replacing a plate frame and lime precipitation step, so that an ultrafiltration process section is omitted; membrane concentration is adopted, so that the evaporation capacity of evaporationand concentration equipment is reduced, the energy consumption is reduced, and a part of inorganic salt is removed; an ion exchange decolorization and impurity removal process is used for replacing astoving process, so that the problem of sulfur residues in cane sugar is solved, and the product quality is improved; ion exchange desalination is adopted, so that salt in the sucrose juice is effectively removed; MVR evaporation and concentration are adopted, so that the energy consumption is effectively reduced.

Description

technical field [0001] The invention belongs to the technical field of sugar production, and in particular relates to a method for refining white granulated sugar. Background technique [0002] my country is one of the major sugar production and consumption countries in the world. There are nearly 300 domestic enterprises engaged in sugar production and processing, with an annual output of nearly 14 million tons of sugar. At present, the commonly used sucrose production processes in my country include "two-step method", sulfurous acid method, and carbonic acid method. [0003] The "two-step method" requires large investment, complicated process, and high production cost, so it is not suitable for promotion in China; the sucrose produced by the carbonic acid method is of good quality, but the process is complicated, the process is long, the investment is large, and the environmental pollution is serious. [0004] Sulfurous acid method is currently the main method of sugar pr...

Claims

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Application Information

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IPC IPC(8): C13B10/02C13B20/16C13B20/14C13B25/00C13B30/00C13B30/02C13B40/00
CPCC13B10/02C13B20/14C13B20/16C13B20/165C13B25/00C13B30/002C13B30/02C13B40/00
Inventor 不公告发明人
Owner 彭冬元
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