Functionalized graphene-based solar back aluminum slurry and preparation method thereof
A technology of solar energy and graphene, applied in the direction of conductive materials dispersed in non-conductive inorganic materials, cable/conductor manufacturing, electrical components, etc., can solve problems such as poor bending resistance, poor adhesion, and poor conductivity , to achieve good weather resistance, excellent printing performance and chemical resistance, good electrical conductivity
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Embodiment 1
[0029] First prepare functionalized graphene dispersion liquid, its process is: Utilize A-187 coupling agent to modify graphene oxide, obtain modified graphene oxide by A-187 coupling agent and graphene oxide reaction: by mass 50 parts of modified graphene oxide were dissolved in 40 parts of a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1. After ultrasonication for 40 min, 5 parts of absolute ethanol with a concentration of 40 g / L containing a coupling agent were placed in the Add slowly under stirring, continue to react for 18 hours after the addition, and wash the obtained pasty product 3 times with absolute ethanol to remove excess coupling agent, then wash 5 times with deionized water, filter, and dry in a 60°C oven ; After modification, covalent bonds are formed between each other to significantly improve the thermal stability of the modified graphene oxide; then it is reduced, and the modified graphene oxide is placed in a ceramic cruci...
Embodiment 2
[0033] First prepare functionalized graphene dispersion liquid, its process is: Utilize A-1100 coupling agent to modify graphene oxide, obtain modified graphene oxide by A-1100 coupling agent and graphene oxide reaction: by mass 50 parts of modified graphene oxide were dissolved in 40 parts of a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1. After ultrasonication for 40 min, 5 parts of absolute ethanol with a concentration of 40 g / L containing a coupling agent were placed in the Add slowly under stirring, continue to react for 18 hours after the addition, and wash the obtained pasty product 3 times with absolute ethanol to remove excess coupling agent, then wash 5 times with deionized water, filter, and dry in a 60°C oven ; After modification, covalent bonds are formed between each other to significantly improve the thermal stability of the modified graphene oxide; then it is reduced, and the modified graphene oxide is placed in a ceramic cru...
Embodiment 3
[0037] First prepare functionalized graphene dispersion liquid, its process is: Utilize A-174 coupling agent to modify graphene oxide, obtain modified graphene oxide by A-174 coupling agent and graphene oxide reaction: by mass 50 parts of modified graphene oxide were dissolved in 40 parts of a mixed solution of deionized water and absolute ethanol with a volume ratio of 1:1. After ultrasonication for 40 min, 5 parts of absolute ethanol with a concentration of 40 g / L containing a coupling agent were placed in the Add slowly under stirring, continue to react for 18 hours after the addition, and wash the obtained pasty product 3 times with absolute ethanol to remove excess coupling agent, then wash 5 times with deionized water, filter, and dry in a 60°C oven ; After modification, covalent bonds are formed between each other to significantly improve the thermal stability of the modified graphene oxide; then it is reduced, and the modified graphene oxide is placed in a ceramic cruci...
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