Clean fracturing fluid with liquid thickening agent and preparation method thereof
A technology of clean fracturing fluid and thickener, applied in the field of fracturing fluid, can solve the problems of increased construction links, viscoelastic damage of fracturing fluid, and reduction of viscoelastic properties of fracturing fluid, so as to improve oil recovery efficiency and reduce formation damage small effect
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Embodiment 1
[0027] Step 1: mixing high-melting-point unsaturated fatty acids with low-melting-point unsaturated fatty acids in a mass ratio of 1:2 to prepare an unsaturated fatty acid thickener;
[0028] Among them, the unsaturated fatty acid with high melting point is erucic acid, and the unsaturated fatty acid with low melting point is oleic acid.
[0029] Step 2: Prepare a strong alkali solution, that is, a mixed aqueous solution of sodium hydroxide and potassium chloride, wherein the mass percentage of sodium hydroxide is 0.8%, and the mass percentage of potassium chloride is 2.2%.
[0030] Step 3: Mix the unsaturated fatty acid thickener in step 1 and the strong alkali solution in step 2 at a mass ratio of 2.4:100 under vigorous stirring to form clean fracturing that can carry sand within 3 minutes Liquid hydrogel, the viscosity at room temperature can reach 70mPa.s, used as fracturing fluid, can withstand the temperature above 50 ℃.
Embodiment 2
[0032] Step 1: mixing high-melting-point unsaturated fatty acids with low-melting-point unsaturated fatty acids at a mass ratio of 1:2.5 to prepare an unsaturated fatty acid thickener;
[0033] Among them, the unsaturated fatty acid with high melting point is erucic acid, and the unsaturated fatty acid with low melting point is oleic acid.
[0034] Step 2: Prepare a strong alkali solution, that is, a mixed aqueous solution of sodium hydroxide and potassium chloride, wherein the mass percentage of sodium hydroxide is 1.0%, and the mass percentage of potassium chloride is 2.6%.
[0035] Step 3: Mix the unsaturated fatty acid thickener in step 1 and the strong alkali solution in step 2 at a mass ratio of 2.7:100 under vigorous stirring to form clean fracturing that can carry sand within 3 minutes Liquid hydrogel, the viscosity at room temperature can reach 65mPa.s, used as fracturing fluid, can withstand the temperature above 50 ℃.
Embodiment 3
[0037] Step 1: mixing high-melting-point unsaturated fatty acids with low-melting-point unsaturated fatty acids at a mass ratio of 1:3 to prepare an unsaturated fatty acid thickener;
[0038] Among them, the unsaturated fatty acid with high melting point is erucic acid, and the unsaturated fatty acid with low melting point is palmitoleic acid.
[0039] Step 2: Prepare a strong alkali solution, that is, a mixed aqueous solution of sodium hydroxide and potassium chloride, wherein the mass percentage of sodium hydroxide is 1.2%, and the mass percentage of potassium chloride is 3%.
[0040] Step 3: Mix the unsaturated fatty acid thickener in step 1 and the strong alkali solution in step 2 at a mass ratio of 3:100 under vigorous stirring to form clean fracturing that can carry sand within 3 minutes Liquid hydrogel, the viscosity at room temperature can reach 65mPa.s, used as fracturing fluid, can withstand the temperature above 50 ℃.
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