A kind of microemulsion non-ferrous metal mold release agent and preparation method thereof
A technology of non-ferrous metal and mold release agent, which is used in the production of micro-emulsion non-ferrous metal mold release agent, and the field of micro-emulsion non-ferrous metal mold release agent, which can solve the problems of contaminated container, poor mold release effect, and unstable emulsification.
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example 1
[0028] Example 1, according to the microemulsion nonferrous metal release agent of the present invention, prepare according to the following steps:
[0029] Polyethylene wax 18 stearyl alcohol 6 primary amine 9 nonanol 3
[0030] Epoxy castor oil 10 additives 5 deionized water 29
[0031] 1) at room temperature, stearyl alcohol and primary amine are mixed and stirred to obtain a co-emulsifier, and nonanol and primary amine are mixed and stirred to obtain a solubilizer;
[0032] 2) Mix the polyethylene wax, co-emulsifier and solubilizer according to the weight ratio of 3:2:1, put it into a stirrer with a rotation speed of 200-300r / min, slowly heat to 70°C, and heat at a constant temperature for 1h , to obtain a uniformly dispersed emulsifier A;
[0033] 3) slowly heating the modified vegetable oil to 50°C;
[0034] 4) Slowly add emulsifier A to the modified vegetable oil ester obtained in step 3), add acetic acid, adjust the pH of the solution to 5, emulsify through phase in...
example 2
[0037] Example 2, prepare microemulsion non-ferrous metal release agent according to the following steps:
[0038] Polyethylene wax 19.5 stearyl alcohol 6.5 primary amine 9.75 nonanol 3.25
[0039] Epoxy butyl furfurate 15 additives 6 deionized water 40
[0040] 1) at room temperature, stearyl alcohol and primary amine are mixed and stirred to obtain a co-emulsifier, and nonanol and primary amine are mixed and stirred to obtain a solubilizer;
[0041] 2) Mix the polyethylene wax, co-emulsifier and solubilizer according to the weight ratio of 3:2:1, put it into a stirrer with a rotation speed of 200-300r / min, stir slowly, heat to 80°C, and heat at constant temperature for 1h , to obtain a uniformly dispersed emulsifier A;
[0042] 3) slowly heating the modified vegetable oil to 55°C;
[0043] 4) Slowly add emulsifier A to the modified vegetable oil ester obtained in step 3), add acetic acid, adjust the pH of the solution to 5, emulsify through phase inversion, stir slowly an...
example 3
[0046] Example 3, prepare microemulsion non-ferrous metal release agent according to the following steps:
[0047] Emulsifier: 38
[0048] Modified vegetable oil: 12
[0049] Auxiliary: 6
[0050] Deionized water: 50
[0051] Polyethylene wax 21 stearyl alcohol 7 primary amine 10.5 nonanol 3.5
[0052] Epoxy butyl oleate 20 additives 10 deionized water 50
[0053] 1) at room temperature, stearyl alcohol and primary amine are mixed and stirred to obtain a co-emulsifier, and nonanol and primary amine are mixed and stirred to obtain a solubilizer;
[0054] 2) Mix the polyethylene wax, co-emulsifier and solubilizer according to the weight ratio of 3:2:1, put it into a stirrer with a rotation speed of 200-300r / min, and slowly heat it to 100°C, and heat it at a constant temperature for 2h , to obtain a uniformly dispersed emulsifier A;
[0055] 3) slowly heating the modified vegetable oil to 60°C;
[0056] 4) Slowly add emulsifier A to the modified vegetable oil obtained in s...
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