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Preparation method of functionalized plant fiber plaster material

A plant fiber and gypsum material technology, applied in the field of building materials, can solve the problems of difficult to control setting time and interface performance, difficult to realize other functions, poor interface performance, etc. Effects of porosity and specific surface area

Inactive Publication Date: 2013-10-02
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In terms of literature: such as Ai Taotao studied the use of MgCl 2 , MgO as cementing material and plant fiber to prepare plant fiber decorative board formula (Ceramics, 2008 No. 8), Zhu Heqing et al. studied the application of plant fiber cement hollow lightweight wallboard in construction (Building wood-based panels, 2001 No. 4), Yang Zijiang et al. studied the plant fiber gypsum slag reinforced block (new wall material, No. 5, 2006)..., analyzing these documents, it can be found that when using plant fibers to prepare building materials, most of them are directly The method of using plant fibers, but when using plant fibers directly, there are generally problems such as easy aging and poor interface properties.
[0005] In terms of patents: there have been contents of direct compounding of gypsum and plant fibers to prepare plant fiber-gypsum composite materials, but analysis of these patents reveals that the plant fibers involved in the relevant claims have not been modified, but directly used, such as Plant fiber gypsum board light steel keel fireproof partition wall (01279630), a preparation method of plant fiber gypsum block (01138351), a production method of plant fiber reinforced and toughened fluorogypsum paper panel (201010545685), etc., using these Methods Plant fibers can be used to obtain certain thermal insulation properties, but other functions are difficult to realize. At the same time, because the surface of plant fibers contains some waxy materials, its setting time and interface properties are difficult to control.

Method used

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  • Preparation method of functionalized plant fiber plaster material
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] The rice straw was thermally analyzed in the STA449C comprehensive analyzer produced by the German Netzsch company at a temperature increase of 5 °C / min, and the ignition point temperature was measured to be 313 °C;

[0027] First place the straw in the N 2 In the atmosphere, the room temperature was raised to 310°C, kept for 30 minutes, and cooled to room temperature, and then 20% of the obtained modified plant fiber was mixed with 70% of β hemihydrate gypsum, 9.99% of lime, and 0.01% of carboxypropyl methyl cellulose ether according to the mass ratio. Mix evenly to get the final product,

[0028] Among them, the β hemihydrate gypsum has a fineness of 0.2mm square hole sieve less than or equal to 15.0wt%, lime has a calcium oxide content greater than or equal to 85wt%, and its fineness of 0.90mm square hole sieve is less than or equal to 1.5wt%. 0.125mm square hole sieve residue is less than or equal to 18.0wt%,

[0029] When in use, add water accounting for 71% of t...

Embodiment 2

[0032] The cornstalk was thermally analyzed in the STA449C comprehensive analyzer produced by the German Netzsch company at a temperature increase of 2°C / min, and its ignition point was measured to be 344°C;

[0033] First put the cornstalks in the O 2 In an atmosphere with a content of <1%, the room temperature is raised to 330°C, the temperature is kept for 120 minutes, and the temperature is lowered to room temperature. Then, according to the mass ratio, 30% of the modified plant fiber obtained is mixed with 60% of β-hemihydrate gypsum, 5% of lime, 4.98% of slag cement, Carboxypropyl methyl cellulose ether 0.02% is evenly mixed to obtain the final product,

[0034] Among them, the β hemihydrate gypsum has a fineness of 0.2mm square hole sieve less than or equal to 15.0wt%, lime has a calcium oxide content greater than or equal to 85wt%, and its fineness of 0.90mm square hole sieve is less than or equal to 1.5wt%. 0.125mm square hole sieve residue is less than or equal to 1...

Embodiment 3

[0037] The straw was thermally analyzed in the STA449C comprehensive analyzer produced by the German Netzsch company at a temperature increase of 5°C / min, and the ignition point temperature was measured to be 344°C;

[0038] First, the bagasse was added to the N 2 In the atmosphere, the room temperature was raised to 340°C, kept for 80 minutes, and then cooled to room temperature, and then 50% of the obtained modified plant fiber was mixed with 40% of β hemihydrate gypsum, 9.96% of ordinary Portland cement, and 0.04% of polyacrylamide according to the mass ratio. Mix to get the final product,

[0039] Among them, the sieve residue of β hemihydrate gypsum with a fineness of 0.2mm square hole sieve is less than or equal to 15.0wt%,

[0040] When in use, add water accounting for 70% of the product mass and stir for 3 minutes. It can be used for pouring and molding of plasterboard. After testing, its thermal conductivity can reach 0.045W / m·K, and the equilibrium moisture content ...

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Abstract

The invention relates to a preparation method of a functionalized plant fiber plaster material. The preparation method comprises the steps of: firstly, conducting semi-carbonization treatment to plant fiber to obtain modified plant fiber, and then evenly mixing the modified plant fiber, a plaster, a water-reducing agent, an air entraining agent, a gas-forming agent, a thickener, lime and cement, to obtain the functionalized plant fiber plaster material. The preparation method has the beneficial effects of being large in waste consumption quantity and strong in product functionality, as well as the advantages that 1) the maximum plant fiber consumption quantity can achieve 50%, thus being conductive to saving resource consumption in the production process of products; 2) after being modified, the plant fiber integrates the toughness and strong adsorbability, the porosity and specific surface area of the material can be increased, from the basic phase (plaster and semi-carbonized fiber) to the internal structure of the material all have certain humidifying and heat-preserving functions, and compared with the existing energy-saving material, the functionalized plant fiber plaster material is high in waste utilization rate, and strong in functionality, and the product can obtain good properties of fracture resistance, moisture absorption, heat preservation and the like.

Description

technical field [0001] The invention specifically relates to a preparation method of a functional plant fiber gypsum material, which is mainly used in the field of building materials. Background technique [0002] my country is a large agricultural country, and the amount of agricultural waste discharged every year is astonishing. According to statistics, the amount of crop straw produced in my country is about 70 million tons every year, and the total amount of straw resources available for collection is as high as 60 million tons every year. After the crops are harvested, in order to ensure the re-cultivation of the land, a large amount of crop stalks are burned, which not only wastes natural resources, but also pollutes the environment, causing CO 2 And PM2.5 seriously exceeded the standard. With the enhancement of people's awareness of environmental protection, the treatment of crop straw has aroused people's high attention. [0003] At present, there have been a lot o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/14C04B18/24C04B38/02
CPCY02W30/91
Inventor 蹇守卫蔡礼雄邢金宇马保国郅真真汪婷王智
Owner WUHAN UNIV OF TECH
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