Preparation method of bacterial-cellulose-fiber-based nano-grade carbon fiber
A technology of bacterial cellulose and carbon nanofibers, which is applied in the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of inability to prepare carbon nanofibers
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Embodiment 1
[0025] Place the bleached bacterial cellulose wet film between a pair of holding rollers with a diameter of 20mm, and feed it at a certain speed (10 mm / min); through a polishing wheel composed of needle-shaped, superhard, and elastic stainless steel wires Needle-like carding on the surface, high-speed puncture, splitting and carding, transforming the bacterial cellulose wet film into bacterial cellulose fibers; the bacterial cellulose ultra-fine fibers are filtered by a filter press to prepare 100% moisture content Bacterial cellulose superfine fiber, superfine fiber diameter 100nm, superfine fiber length 40mm; the above bacterial cellulose superfine fiber is treated with liquid nitrogen, put into a vacuum freeze dryer to freeze-dry, and after the fiber does not contain moisture, Prepare the porous bacterial cellulose superfine dry fiber with the macroscopic appearance and constant volume when the wet state is maintained; the above superfine fiber is placed in a muffle furnace,...
Embodiment 2
[0027] Place the bleached bacterial cellulose wet film between a pair of holding rollers with a diameter of 50mm, and feed it at a certain speed (50mm / min); through a polishing wheel composed of needle-shaped, superhard, and elastic stainless steel wires Needle-like carding on the surface, high-speed puncture, splitting and carding, transforming the bacterial cellulose wet film into bacterial cellulose fibers; the bacterial cellulose ultra-fine fibers are filtered by a filter press to prepare 100% moisture content Bacterial cellulose superfine fiber, the diameter of the superfine fiber is less than 100nm, and the length of the superfine fiber is less than 60mm; after the above bacterial cellulose superfine fiber is treated with liquid nitrogen, it is placed in a vacuum freeze dryer and freeze-dried until the fiber does not contain moisture Finally, the porous bacterial cellulose superfine dry fiber with the macroscopic appearance and constant volume in the wet state is prepared...
Embodiment 3
[0029]Place the bleached bacterial cellulose wet film between a pair of holding rollers with a diameter of 80mm, and feed it at a certain speed (1000 mm / min); through a polishing wheel composed of needle-shaped, superhard, and elastic stainless steel wires Needle-like carding on the surface, high-speed puncture, splitting and carding, transforming the bacterial cellulose wet film into bacterial cellulose fibers; the bacterial cellulose ultra-fine fibers are filtered by a filter press to prepare 90% moisture content Bacterial cellulose superfine fiber, the diameter of the superfine fiber is less than 100nm, and the length of the superfine fiber is less than 100mm; after the above bacterial cellulose superfine fiber is treated with liquid nitrogen, it is placed in a vacuum freeze dryer to freeze-dry, and the fiber does not contain moisture Finally, the porous bacterial cellulose superfine dry fiber with the macroscopic appearance and constant volume in the wet state is prepared; ...
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