Chewing gum containing sweet tea extract and preparation method thereof
A technology of sweet tea extract and chewing gum, applied in the field of chewing gum, can solve the problems such as the decrease of inhibition effect, and achieve the effect of preventing the generation of dental plaque
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Embodiment 1
[0022] The formula of chewing gum containing sweet tea extract: 10% sweet tea extract, 90% gum base; wherein, rubusoside accounts for 40% of the weight of sweet tea extract, and sweet tea polyphenols accounts for 21% of the weight of sweet tea extract.
[0023] 1) Take sweet tea leaves and crush them to 40 meshes, put them into 30% (v / v) ethanol, reflux and extract twice under ultrasonic wave 40KHz, temperature 40°C, extract 20min each time, combine the extracts, filter, and take the filtrate The solvent is recovered to obtain the crude extract of sweet tea.
[0024] 2) Add lime water to the crude sweet tea extract to make the pH value 9, after impurities precipitate, filter out the precipitate, and take the supernatant for later use.
[0025] 3) After adjusting the pH of the supernatant to neutral, use D101 macroporous adsorption resin for adsorption separation, elute with 70% (v / v) ethanol, take the eluate to concentrate, dry, and it is the sweet tea extract , wherein the w...
Embodiment 2
[0027] The formula of the chewing gum containing sweet tea extract: sweet tea extract 0.2%, gum base 99.8%; wherein, rubusoside accounts for 5% of sweet tea extract weight, sweet tea polyphenol accounts for 2% of sweet tea extract weight.
[0028] The preparation method of described sweet tea extract:
[0029] Take sweet tea leaves and grind them to 5 mesh, put them into 80°C water and extract twice, each time for 20 minutes, combine the extracts, filter, concentrate, and dry to obtain sweet tea extracts, wherein the weight content of rubusoside is 5% , The weight content of sweet tea polyphenols is 2%.
Embodiment 3
[0031] The formula of the chewing gum containing sweet tea extract: sweet tea extract 10%, gum base 90%; wherein, rubusoside accounts for 5% of sweet tea extract weight, sweet tea polyphenol accounts for 21% of sweet tea extract weight.
[0032] The preparation method of described sweet tea extract:
[0033] 1) Take sweet tea leaves and crush them to 20 meshes, put them in 10% (v / v) ethanol, extract them twice at room temperature for 20 minutes each time, combine the extracts, filter, take the filtrate to recover the solvent, and obtain crude sweet tea extracts thing.
[0034] 2) Adsorb and separate the sweet tea crude extract with D101 macroporous adsorption resin, elute with 50% (v / v) ethanol, take the eluate to concentrate, dry, and it is the sweet tea extract. Among them, the weight content of rubusoside 5%, and the weight content of sweet tea polyphenols is 21%.
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