Tombarthite luminescent material, preparation method and application thereof
A rare earth luminescence and luminescence material technology, applied in the field of luminescence and detection, can solve the problems of long luminescence life and low luminescence efficiency, and achieve the effects of short fluorescence life, simple preparation method and high product density
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Embodiment 1
[0023] Weigh lithium carbonate (Li 2 CO 3 ) 0.09 g, tungsten trioxide (WO 3 ) 1.16 g, lutetium trioxide (Lu 2 O 3 ) 0.49 g and tetraterbium heptaoxide (Tb 4 O 7 ) 0.01 g, grind well in an agate mortar, put it into a quartz crucible, heat it in an air bath in a high-temperature furnace to a constant temperature of 600°C for 2 hours, then raise it to a constant temperature of 1000°C for 8 hours, cool naturally and grind into a powder to obtain the final product .
Embodiment 2
[0025] Weigh sodium carbonate (Na 2 CO 3 ) 0.13 g, tungsten trioxide (WO 3 ) 1.16 g, lutetium trioxide (Lu 2 O 3 ) 0.48 g and tetraterbium heptaoxide (Tb 4 O 7 ) 0.01 g, grind well in an agate mortar, put it in a quartz crucible, heat it in an air bath in a high-temperature furnace to a constant temperature of 500°C for 4 hours, then raise it to a constant temperature of 1000°C for 4 hours, and grind it into a powder after natural cooling. .
Embodiment 3
[0027] Weigh potassium carbonate (K 2 CO 3 ) 0.17 g, tungsten trioxide (WO 3 ) 1.16 g, lutetium trioxide (Lu 2 O 3 ) 0.47 g and tetraterbium heptaoxide (Tb 4 O 7 ) 0.02 g, grind well in an agate mortar, put it into a quartz crucible and heat it in an air bath in a high-temperature furnace to a constant temperature of 500°C for 6 hours, then raise it to a constant temperature of 1000°C for 3 hours, and grind into a powder after natural cooling to obtain the final product .
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