Polymer film and its application in a lighting assembly
A technology of polymer film and light-emitting device, which is applied in parts of lighting devices, semiconductor devices of light-emitting elements, lighting devices, etc., can solve the problems of yellowing, high reflectivity, low penetration, etc., and achieve improvement of yellowing , High reflectivity, low penetration effect
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[0038] Preparation of polyimide film
Synthetic example 1
[0040] Nitrogen gas was fed into a 500 milliliter (ml) three-necked flask as the polymerization vessel at ambient temperature. All reactions were performed under nitrogen atmosphere. About 160 grams (g) of dimethylacetamide (DMAC) as solvent was added to the flask. About 18.774 g (0.060 mole) of 2,2'-bis(trifluoromethyl)benzidine (TMFB) was dissolved in DMAC. After TMFB is completely dissolved in DMAC, add about 13.354g (0.045moles) of biphenyltetracarboxylic dianhydride (BPDA) and about 7.873g (0.015moles) of 2,2-bis[4-(dicarboxyphenoxy ) phenyl] propane dianhydride dianhydride (BPADA) to the solution, and add 8.411g of titanium dioxide (TiO 2 ) slurry (the solid content of the slurry is about 50%), and the stirring is continued for about 4 hours to form a polyamic acid (PAA) solution.
[0041] The obtained PAA solution was mixed with an acetic anhydride dehydrating agent and a picoline catalyst to obtain a precursor solution. Then, on a glass plate, the precursor so...
Synthetic example 2
[0043] Compared with Synthesis Example 1, the difference of Synthesis Example 2 is that 25.833g of titanium dioxide slurry (solid content of the slurry is about 50%) was added, and the rest of the preparation process was the same as Synthesis Example 1 to form a white polyimide film.
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