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Flame-retardation enhanced epoxy plastic sheet material and its preparation method

A technology of epoxy plastics and plates, applied in the field of polymer material modification and processing, can solve the problems of high cost, high price, unfavorable development of the automobile industry, etc., and achieve the effect of low cost, long life and low cost

Active Publication Date: 2013-01-16
九江鑫星绝缘材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But this material is an imported material, the price is high and the cost is high, which is not conducive to popularization and the development of the automobile industry

Method used

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  • Flame-retardation enhanced epoxy plastic sheet material and its preparation method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] Add 100 parts of epoxy resin, 8 parts of dioctyl phthalate, 5 parts of EPDM rubber, 100 parts of glass fiber, 30 parts of quartz powder, and 10 parts of allyl glycidyl ether into the reaction kettle according to the formula ratio , stirring at 70°C for 10 minutes;

[0040] Add 20 parts of chlorinated paraffin and 5 parts of antimony trioxide into the above mixture, heat to 80°C, and stir until no solid particles appear; then add 9 parts of diethylenetriamine-propylene oxide phenyl ether adduct , stir well;

[0041] Put the prepared material liquid under vacuum (vacuum degree is 9.5*10 4 Pa) Stirring, the stirring speed is 180r / min, degassing for 12 minutes; then the degassed material is placed in a molding mold for curing, and it is released after 3.5 hours, and the mold temperature is 90°C;

[0042] Then, the above-mentioned board after release was kept at a constant temperature of 55° C. for 2 hours. The obtained plates were processed into test specimens according ...

Embodiment 2

[0044] Add 100 parts of epoxy resin, 14 parts of dibutyl phthalate, 8 parts of nitrile rubber, 80 parts of glass fiber, 20 parts of calcium carbonate, and 12 parts of allyl glycidyl ether into the reactor according to the formula ratio. Stir at 75°C for 8 minutes;

[0045] Add 15 parts of decabromodiphenyl ether and 6 parts of zinc borate into the above mixture, heat to 85°C, and stir until no solid particles appear; then add 5 parts of 2-methylimidazole, and stir to mix;

[0046] Put the prepared material liquid under vacuum (vacuum degree is 9.2*10 4 Pa) Stirring at a stirring speed of 170r / min, degassing for 10 minutes; then placing the degassed material in a molding mold for curing, and releasing it after 3 hours, and the mold temperature is 80°C;

[0047] Then, the above-mentioned board after release was kept at a constant temperature of 60° C. for 1.5 hours. The obtained plates were processed into test specimens according to the standard experimental requirements, and ...

Embodiment 3

[0049] Add 100 parts of epoxy resin, 6 parts of dinonyl phthalate, 4 parts of EPDM rubber, 120 parts of glass fiber, 60 parts of calcium carbonate, and 8 parts of allyl glycidyl ether into the reaction kettle according to the formula ratio , stirred at 80°C for 8 minutes;

[0050] Add 20 parts of tetrabromobisphenol A and 6 parts of antimony trioxide into the above mixture, heat to 95°C, and stir until no solid particles appear; then add 10 parts of diethylenetriamine-propylene oxide phenyl ether adduct portion, stir well;

[0051] Put the prepared material liquid under vacuum (vacuum degree is 10.0*10 4 Pa) Stirring at a stirring speed of 160r / min, degassing for 14 minutes; then placing the degassed material in a molding mold for curing, and releasing it after 3 hours, and the mold temperature is 100°C;

[0052] Then, the above-mentioned board after release was kept at a temperature of 65° C. for 2 hours at a constant temperature. The obtained plates were processed into te...

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Abstract

The invention belongs to the technical field of high-molecular material modification and processing and discloses a flame-retardation enhanced epoxy plastic sheet material and its preparation method. The epoxy plastic sheet material comprises the following ingredients of: by weight, 100 parts of epoxy resin, 5-20 parts of a plasticizer, 3-15 parts of a flexibilizer, 80-150 parts of reinforced fibers, 0-100 parts of a filler, 8-15 parts of a diluent, 15-30 parts of a fire retardant, 3-8 parts of a flame-retardation synergistic agent and 5-18 parts of a curing agent. In comparison with the prior art, the flame-retardation enhanced epoxy plastic sheet material provided by the invention has advantages of strong strength, good toughness, impact resistance, long service life, low cost, flame retardation and good flame resistance, is easy to process, and can meet the criteria at V-0 level of UL-94. The material provided by the invention can be widely applied in many national economical fields such as automobile, building sheet material and the like.

Description

technical field [0001] The invention belongs to the technical field of polymer material modification and processing, and relates to an epoxy plastic plate and a preparation method thereof. Background technique [0002] With the development of the automobile industry, my country's automobile production has grown steadily, and the scale of automobile consumption has become increasingly large. According to data released by the China Association of Automobile Manufacturers, my country's output reached 9.3451 million vehicles in 2008, and the sales volume of automobiles reached 9.3805 million vehicles. Although the global economic crisis has had a serious impact on the auto industries of various countries, domestic auto manufacturers have actively responded, and with the support of government policies, China's auto sales have recently begun to pick up. From the perspective of the overall trend, my country's auto industry will still maintain a stable Sustained rapid growth. While...

Claims

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Application Information

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IPC IPC(8): C08L63/00C08L63/02C08L63/04C08L77/00C08L9/02C08L23/16C08K13/04C08K5/12C08K7/14C08K7/06C08K7/12
Inventor 郭学林
Owner 九江鑫星绝缘材料有限公司
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