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Method for producing soap powder by illegal cooking oil

A technology of waste oil and soap powder, which is applied in the direction of chemical instruments and methods, soap solution manufacturing, mixing/kneading soap, etc., can solve the problems of difficult reuse of waste acid water, low yield of crude fatty acid, and influence on the surrounding environment, etc., to achieve Delicate and smooth touch, good reduction, environmental protection effect

Inactive Publication Date: 2012-12-05
杨解定
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1) The acidification process adopts the open flame heating method. The acidification process emits odor and affects the surrounding environment. It is difficult to reuse waste acid water and directly affects groundwater, lakes and other water bodies.
[0005] 2) The hydrolysis process adopts the atmospheric pressure hydrolysis method. During the hydrolysis process, other catalysts need to be added, and the time needs to be more than 20 hours. After hydrolysis, the acid value of black fatty acid is low, resulting in a low yield of crude fatty acid
[0007] 4) The agglomeration method is adopted in the production of soap powder, and the solubility of soap powder is poor
[0008] 5) Refined fatty acids of soap powder raw materials need to be transported and heated, resulting in increased production costs

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:

[0026] 1) Add 10% water to the waste oil after impurity removal, stir and heat to 86°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, then stir for 35 minutes, and let stand to separate after the reaction , to separate the liquid;

[0027] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 7.0, and then let it stand for stratification;

[0028] 3) According to the oil-water ratio of 3:2, put it into the hydrolysis tower for heating. When the pressure is 0.7MPa, the pressure is slightly relieved and exhausted. When the pressure is 0.8MPa, the acid value is 120mgKOH / g, and the time is 12 hours. 0.1MPa, take out the material, let it stand for stratification, and drain the lower layer of water to obtain black fatty acid, and obtain refined mixed fatty acid after dehydration distillation...

Embodiment 2

[0032] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:

[0033] 1) Add 8% water to the waste oil after impurity removal, stir and heat to 80°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, and then stir for 30 minutes. layers, separating liquids;

[0034] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 8.0, and then let it stand for stratification;

[0035] 3) According to the oil-water ratio of 3:2, put it into the hydrolysis tower for heating, and release the pressure slightly when the pressure is 0.6MPa. When the pressure is 0.8MPa, the acid value is 140mgKOH / g, and the time is 10 hours; if the acid value is 160mgKOH / g , the time is 8 hours, after the reaction is completed, the pressure is reduced to 0.1MPa, the material is taken out, the lower layer of water is discharged after standing for stratification, and the black fatty acid...

Embodiment 3

[0039] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:

[0040] 1) Add 12% water to the waste oil after impurity removal, stir and heat to 90°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, and then stir for 40 minutes. After the reaction is complete, let it stand for stratification , to separate the liquid;

[0041] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 7.5, and then let it stand for stratification;

[0042] 3) Put it into the hydrolysis tower for heating according to the ratio of oil to water 3:2, and slightly release the pressure to exhaust when the pressure is 0.8MPa. When the pressure is 0.8MPa, the acid value is 160mgKOH / g, the time is 8 hours, and the pressure is reduced after the reaction is completed. to 0.1MPa, take out the material, let it stand for stratification, and drain the lower layer of water to obtain blac...

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PUM

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Abstract

The invention discloses a method for producing soap powder by illegal cooking oil. The method comprises the steps as follows: 1) adding water into the illegal cooking oil after impurity removal, stirring for heating, slowly dropwise adding concentrated sulfuric acid, after the reaction is ended, standing for layering, and separating liquid; 2) washing an oil layer by water, and standing for layering; 3) driving into a hydrolysis tower according to the oil-to-water ratio for heating, slightly relieving pressure for exhausting when the pressure is 0.6-0.8 MPa, after the reaction is ended, reducing the pressure to be 0.l MPa, taking out a material, standing for layering, discharging the underlying water to obtain black fatty acid, and carrying out dehydration, distillation and multi-tower distillation to obtain refined mixed fatty acid; 4) adding sodium hydroxide, sodium carbonate, sodium silicate, sodium sulfate, 4A zeolite and carboxymethylcellulose into the refined mixed fatty acid, ageing in an ageing kettle, and conveying into a powder spraying tower through a homogenizing pump and a high pressure pump; and 5) drying into a powder shape through hot air in the powder spraying tower, carrying out settling separation, sieving, lifting into a mixing tank, adding protease, a non-ionic surface active agent and spice, and uniformly mixing. The method has the advantages of simple process, no pollution, low cost and resource conservation.

Description

technical field [0001] The invention relates to a method for producing soap powder, in particular to a method for producing soap powder by using waste oil. Background technique [0002] With the rapid development of social economy, hotels, hotels and other various catering institutions are expanding day by day, the number is increasing rapidly, and the amount of waste water is also increasing. Most oily sewage contains more floating and suspended matter , some even contain a large amount of impurities such as silt and leftover food, and the waste water is directly discharged into the sewer, which not only pollutes the surrounding environment, but also often causes the sewer to be blocked due to the solidification of grease in winter, and the sewage overflows, which not only pollutes the production and living environment , And it also increases unnecessary dredging expenses, the pollutants in its wastewater include chemical oxygen demand COD, BOD, SS animals and plants, and d...

Claims

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Application Information

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IPC IPC(8): C11D13/00C11D13/10C11D9/02C11D9/60C11D17/06
Inventor 杨解定张有谊杨宝玉
Owner 杨解定
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