Method for producing soap powder by illegal cooking oil
A technology of waste oil and soap powder, which is applied in the direction of chemical instruments and methods, soap solution manufacturing, mixing/kneading soap, etc., can solve the problems of difficult reuse of waste acid water, low yield of crude fatty acid, and influence on the surrounding environment, etc., to achieve Delicate and smooth touch, good reduction, environmental protection effect
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Embodiment 1
[0025] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:
[0026] 1) Add 10% water to the waste oil after impurity removal, stir and heat to 86°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, then stir for 35 minutes, and let stand to separate after the reaction , to separate the liquid;
[0027] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 7.0, and then let it stand for stratification;
[0028] 3) According to the oil-water ratio of 3:2, put it into the hydrolysis tower for heating. When the pressure is 0.7MPa, the pressure is slightly relieved and exhausted. When the pressure is 0.8MPa, the acid value is 120mgKOH / g, and the time is 12 hours. 0.1MPa, take out the material, let it stand for stratification, and drain the lower layer of water to obtain black fatty acid, and obtain refined mixed fatty acid after dehydration distillation...
Embodiment 2
[0032] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:
[0033] 1) Add 8% water to the waste oil after impurity removal, stir and heat to 80°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, and then stir for 30 minutes. layers, separating liquids;
[0034] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 8.0, and then let it stand for stratification;
[0035] 3) According to the oil-water ratio of 3:2, put it into the hydrolysis tower for heating, and release the pressure slightly when the pressure is 0.6MPa. When the pressure is 0.8MPa, the acid value is 140mgKOH / g, and the time is 10 hours; if the acid value is 160mgKOH / g , the time is 8 hours, after the reaction is completed, the pressure is reduced to 0.1MPa, the material is taken out, the lower layer of water is discharged after standing for stratification, and the black fatty acid...
Embodiment 3
[0039] A kind of method utilizing waste oil to produce soap powder, comprises the following steps:
[0040] 1) Add 12% water to the waste oil after impurity removal, stir and heat to 90°C, then slowly add 2.0% concentrated sulfuric acid dropwise until the pH value is 2.5, and then stir for 40 minutes. After the reaction is complete, let it stand for stratification , to separate the liquid;
[0041] 2) Wash the oil layer with water at the same temperature as the oil temperature until the pH is greater than 7.5, and then let it stand for stratification;
[0042] 3) Put it into the hydrolysis tower for heating according to the ratio of oil to water 3:2, and slightly release the pressure to exhaust when the pressure is 0.8MPa. When the pressure is 0.8MPa, the acid value is 160mgKOH / g, the time is 8 hours, and the pressure is reduced after the reaction is completed. to 0.1MPa, take out the material, let it stand for stratification, and drain the lower layer of water to obtain blac...
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