High-concentration liquid boric fertilizer and preparation method thereof
A production method and high-concentration technology, applied in fertilization devices, fertilizer mixtures, applications, etc., can solve the problems of low utilization rate and poor water solubility of boron fertilizers, and achieve the effects of low raw material cost, fast dissolution, and good promotion prospects
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specific Embodiment approach 1
[0017] A high-concentration liquid boron fertilizer and a preparation method thereof, comprising the following steps:
[0018] 1. Saponification of fats and oils: add 32kg of meal waste oil to the reaction tank, add 17kg of sodium hydroxide and 41kg of water (weight ratio 1:0.53:1.28), and heat it to 100°C under stirring. Saponification reaction for 2-3 hours, cooling and static layering, removal of the upper layer of higher fatty acid salts, the lower layer of alkaline glycerin mother liquor.
[0019] 2. Boric acid complexation reaction: Separate and take out 54kg of glycerin mother liquor in the above a, add 46kg of boric acid under stirring, turn on the heating coil steam, heat to 90~100℃, stir for 1-1.5 hours, and let stand to cool.
[0020] 3. Adjust the pH value: adjust the pH value of the reaction solution in b above to 7~8 with an appropriate amount of acid and alkali, let it stand for cooling, and quantitatively pack it to form a high-concentration quick-dissolving li...
specific Embodiment approach 2
[0023] A high-concentration liquid boron fertilizer and a preparation method thereof, comprising the following steps:
[0024] 1. Saponification of oil: Add 36kg of meal waste oil to the reaction tank, add 18kg of potassium hydroxide and 46kg of water, (weight ratio 1:0.5:1.27), heat it with steam to 100°C under stirring, and saponify React for 2 to 3 hours, cool and stand still to separate layers, remove the upper layer of higher fatty acid salts, and the lower layer is alkaline glycerin mother liquor.
[0025] 2. Boric acid complexation reaction: Separate and take out 53kg of glycerin mother liquor in the above a, add 47kg of boric acid under stirring, turn on the heating coil steam, heat to 90~100℃, stir for 1-1.5 hours, and let stand to cool.
[0026] 3. Adjust the pH value: adjust the pH value of the reaction solution in b above to 7~8 with an appropriate amount of acid and alkali, let it stand for cooling, and quantitatively pack it to form a high-concentration quick-dis...
specific Embodiment approach 3
[0028] A high-concentration liquid boron fertilizer and a preparation method thereof, comprising the following steps:
[0029] 1. Saponification of oil: Add 42kg of meal waste oil to the reaction tank, add 20kg of potassium hydroxide and 48kg of water, (weight ratio 1:0.47:1.14), heat it to 100°C with steam under stirring, and saponify React for 2 to 3 hours, cool and stand still to separate layers, remove the upper layer of higher fatty acid salts, and the lower layer is alkaline glycerin mother liquor.
[0030] 2. Boric acid complexation reaction: Separate and take 53.5kg of glycerin mother liquor in the above a, add 46.5kg of boric acid under stirring, turn on the heating coil steam, heat to 90~100℃, stir for 1-1.5 hours, and let stand to cool.
[0031] 3. Adjust the pH value: adjust the pH value of the reaction solution in b above to 7~8 with an appropriate amount of acid and alkali, let it stand for cooling, and quantitatively pack it to form a high-concentration quick-di...
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