High-softening-point coal-tar pitch production method
A technology of high softening point asphalt and its production method, which is applied in the direction of processing tar pitch/petroleum pitch/natural pitch by chemical methods, processing tar pitch/petroleum pitch/natural pitch by distillation, etc., which can solve uneven oxidation and difficulty in discharging , Low oxidation efficiency and other issues, to achieve the effect of simple production process, less impurity content and high purity
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Embodiment 1
[0021] Add low-QI purified coal tar pitch into the stirring tank, and continuously feed air, stir during the ventilation process, and carry out air oxidation at 250°C for 6 hours; then add the oxidized pitch to the thin film evaporator , under the conditions of 320°C and vacuum negative pressure of 0.06MPa, thin-film distillation is carried out to remove light components. After distillation for 2 hours, the distillation process is completed to obtain high softening point pitch. The softening point of the obtained high softening point coal tar pitch is 270-290°C , coking value ≥ 70%, QI ≤ 25%, reaching the expected product standard.
Embodiment 2
[0023] Add low-QI purified coal tar pitch into the stirring tank, and continuously feed air, stir during the ventilating process, and carry out air oxidation at 260°C for 6.5 hours; then add the oxidized pitch to the thin film evaporator In the process, thin-film distillation is carried out under the conditions of 330°C and vacuum negative pressure of 0.07MPa to remove light components. After the distillation time is 2.5h, the distillation process is completed to obtain high softening point pitch. The softening point of the obtained high softening point coal tar pitch is 270~ 290℃, coking value ≥ 70%, QI ≤ 25%, reaching the expected product standard.
Embodiment 3
[0025] Add low-QI purified coal tar pitch into the stirring tank, and continuously feed air, stir during the ventilation process, and carry out air oxidation at 270°C for 7 hours; then add the oxidized pitch to the thin film evaporator , under the conditions of 340°C and vacuum negative pressure of 0.08MPa, thin-film distillation is carried out to remove light components, and the distillation time is 3h. After the distillation process is completed, high softening point pitch is obtained. The softening point of the obtained high softening point coal tar pitch is 270-290°C. Coking value ≥ 70%, QI ≤ 25%, reaching the expected product standard.
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