Method for treating nitrobenzene waste water
A technology for nitrobenzene wastewater and wastewater, applied in natural water treatment, chemical instruments and methods, water/sewage multi-stage treatment, etc., to achieve the effect of realizing reuse and avoiding pollution
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Embodiment 1
[0054] Take 100mL of nitrobenzene wastewater, add 4-9g of sodium sulfite to it respectively, dissolve and heat to 40°C, add 10mL of acetone, react for 30min and then raise the temperature to 80°C, add 20mL of formaldehyde solution, continue the reaction for 1h, keep the temperature and add nitric acid 950 parts of base benzene waste water, the effective concentration 0.5% coal-water slurry additive that reacts 1 hour to make; Natural cooling to room temperature, its different molecular weight distribution curves are as follows: figure 1 As shown, the molecular weight of the product decreases significantly with the increase of the amount of sulfonating agent. Wherein the occurrence of sodium sulfite being 4g causes the hydrophilicity of the product to decrease due to insufficient sulfonation, forming a light yellow insoluble matter.
[0055] The non-sticky coal is ground by a ball mill to obtain coal powder with an average particle size of less than 75 μm and the mass percentag...
Embodiment 2
[0057] Take 100mL of nitrobenzene wastewater, add 5g of sodium sulfite to it respectively, dissolve and heat to 40°C, add 6-14mL of acetone, react for 30min and then raise the temperature to 80°C, add 20mL of formaldehyde solution, continue the reaction for 1h, keep the temperature and add nitric acid 950 parts of base benzene waste water, the effective concentration 0.5% coal-water slurry additive that reacts 1 hour to make; Natural cooling to room temperature, its different molecular weight distribution curves are as follows: figure 2 As shown, with the increase of the amount of acetone, the molecular weight of the product first increases and then decreases. When the amount of acetone is small, the molecular weight may be small due to excessive sulfonation, and the initial reaction rate is low; and when the amount of acetone is large, the reaction rate is too fast, and the large ketone-aldehyde ratio is likely to cause a reduction in the degree of polymerization, so that Mo...
Embodiment 3
[0060] Take 100mL of nitrobenzene wastewater, add 5g of sodium sulfite to it respectively, dissolve and heat to 40°C, add 10mL of acetone, react for 30min and then heat up to 80°C, add 12-24mL of formaldehyde solution, continue the reaction for 1h, then keep the temperature and add nitric acid 950 parts of base benzene waste water, the effective concentration 0.5% coal-water slurry additive that reacts 1 hour to make; Natural cooling to room temperature, its different molecular weight distribution curves are as follows: image 3 As shown, with the increase of the amount of formaldehyde, the molecular weight distribution of the product has a greater impact.
[0061] The non-sticky coal is ground by a ball mill to obtain coal powder with a mass percentage of particles with an average particle size of less than 75 μm greater than 80%, and the coal-water slurry additive obtained by reacting 20 ml of formaldehyde and the non-sticky coal powder are mixed according to a mass ratio of ...
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