Method for preparing cobalt-zinc ferrite/polypyrrole nano composite material

A technology of pyrrole nanometer and composite material, which is applied in the directions of cobalt oxide/cobalt hydroxide, iron oxide/iron hydroxide, etc., to achieve the effects of simple process operation, broad application prospect and strong magnetic properties

Inactive Publication Date: 2011-08-24
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology uses an onsite reaction technique for creating small particles called micron spheroids that contain tiny metal pigments attached at their surfaces or inside them. These minute metallic objects help make plasmonics work better than traditional methods like adding other substances into solutions they're meant to protect from harmful radiation. They also enhance certain characteristics such as magnetism (magnitude) and electricity conduction. Overall this new material offers technical benefits over existing technologies due its high efficiency and ease of manufacturing compared to current techniques.

Problems solved by technology

This patents discuss how iron oxide particles can be used in various industries like electronics or energy storage devices due to its unique characteristics including strong resistance against corrosion, ease of manufacturing, durability over time, etc., along with being highly sensitive towards external stimuli like light waves. However, current methods are limited in terms of producing these special types of metal compounds without affecting other qualities associated with them.

Method used

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  • Method for preparing cobalt-zinc ferrite/polypyrrole nano composite material
  • Method for preparing cobalt-zinc ferrite/polypyrrole nano composite material
  • Method for preparing cobalt-zinc ferrite/polypyrrole nano composite material

Examples

Experimental program
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Effect test

Embodiment 1

[0034] (1) Weigh 1.3518g of ferric chloride hexahydrate, 0.3765g of cobalt nitrate hexahydrate, and 0.3722g of zinc nitrate hexahydrate into a 200ml beaker, then add 60ml of ethylene glycol, and stir mechanically at room temperature for 35min. Then add 1.6415g of anhydrous sodium acetate and 1.5ml of polyethylene glycol 200, and ultrasonically disperse for 30 minutes. After it is completely dissolved, pour the above solution into the reaction kettle, raise the temperature to 180°C, and react for 30 hours. After the reaction, the product was collected with a magnet, washed with deionized water and absolute ethanol, and then dried in vacuum at 70°C for 24 hours to obtain Co 0.5 Zn 0.5 Fe 2 o 4 Nano microsphere powder;

[0035] (2) Dissolve 0.7018g sodium dodecylbenzenesulfonate in 200ml deionized water to form an emulsion, add 0.2014g of the above Co 0.5 Zn 0.5 Fe 2 o 4 Nano microsphere powder, stir evenly, and ultrasonically disperse, so that the surfactant and Co 0.5 Z...

Embodiment 2

[0039] (1) Weigh 1.3512g of ferric chloride hexahydrate, 0.5819g of cobalt nitrate hexahydrate, and 0.1488g of zinc nitrate hexahydrate into a 200ml beaker, then add 55ml of ethylene glycol, and stir mechanically at room temperature for 45min. Then add 4.0110g of anhydrous sodium acetate and 1ml of polyethylene glycol 400, and ultrasonicate the mixture for 40 minutes. After it is completely dissolved, pour the above solution into the reaction kettle, raise the temperature to 210°C, and react for 18 hours. At the end of the reaction, the product was collected with a magnet, and the product was washed with deionized water and absolute ethanol, and then the product was vacuum-dried at 80 ° C for 20 h to obtain Co 0.8 Zn 0.2 Fe 2 o 4 Nano microsphere powder;

[0040] (2) Dissolve 0.6054g sodium dodecylbenzenesulfonate in 200ml deionized water to form an emulsion, add 0.2018g of the above Co 0.8 Zn 0.2 Fe 2 o 4 Nano microsphere powder, stir evenly, and ultrasonically dispers...

Embodiment 3

[0044] (1) Weigh 1.3523g of ferric chloride hexahydrate, 0.4134g of cobalt nitrate hexahydrate, and 0.2978g of zinc nitrate hexahydrate into a 200ml beaker, then add 50ml of ethylene glycol, and stir mechanically at room temperature for 40min. Then add 6.017g of anhydrous sodium acetate and 1ml of polyethylene glycol 800, and ultrasonicate the mixture for 50min. After it is completely dissolved, pour the above solution into the reaction kettle, raise the temperature to 190°C, and react for 26h. At the end of the reaction, the product was collected with a magnet, and the product was washed with deionized water and absolute ethanol, and then the product was vacuum-dried at 90°C for 18h to obtain Co 0.6 Zn 0.4 Fe 2 o 4 Nano microsphere powder;

[0045] (2) Dissolve 0.5025g sodium dodecylbenzenesulfonate in 200ml deionized water to form an emulsion, add 0.2010g of the above Co 0.6 Zn 0.4 Fe 2 o 4 Nano microsphere powder, stir evenly, and ultrasonically disperse, so that the...

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Abstract

The invention relates to a method for preparing a cobalt-zinc ferrite/polypyrrole nano composite material, which comprises: (1) dispersing an iron salt, a cobalt salt and a zinc salt into aqueous solution of glycol, adding polyethylene glycol and anhydrous sodium acetate, heating, reacting completely, cooling to room temperature, collecting obtained product by using magnet, washing and drying to obtain cobalt-zinc ferrite (Co1-xZnxFe2O4) nano microsphere powder; (2) preparing suspension of Co1-xZnxFe2O4 nano microspheres subjected to surface modification; and (3), adding a pyrrole monomer andferric chloride into the suspension of the Co1-xZnxFe2O4 nano microspheres subjected to surface modification, and after the reaction is finished, filtering under reduced pressure, washing, drying andobtaining the cobalt-zinc ferrite/polypyrrole nano composite material. In the method, the cost is low, the process operation is simple, needed production equipment is cheap and readily available, andindustrial production can be realized easily. And the nano composite material prepared by the method has high magnetic performance and conductivity and is very practical.

Description

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Claims

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Application Information

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Owner DONGHUA UNIV
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