Production method of water-soluble licoflavone
A technology of licorice flavonoids and production method, which are applied in directions such as pharmaceutical formulations, preparations for skin care, cosmetics, etc., can solve problems such as low solubility, compatibility and application limitations, and achieve the effects of simple operation, simple method and reduced preparation cost.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0015] In a 500mL reaction flask with a stirring and heating reflux device, first add 250g of absolute ethanol and 50g of licorice flavonoids with a purity of 40%, stir to dissolve all the licorice flavonoids, then slowly add 400g of β-cyclodextrin, and the internal temperature rises to 50°C , and stirred for 1 hour. Make cyclodextrin fully include licorice flavonoids. Then dry at 70-80°C under a vacuum condition of -0.09MPa, steam until the clathrate has no ethanol smell, and obtain a reddish-yellow, dry clathrate. The inclusion compound was dissolved in 750 g of deionized water and fully stirred for about 1 hour, filtered, the filtrate was collected, and distilled to a water-soluble flavonoid with a concentration of licorice flavonoids of 2.0% and a reddish-brown color.
Embodiment 2
[0017] In a 500mL reaction flask with a stirring and heating reflux device, first add 250g of absolute ethanol and 50g of licorice flavonoids with a purity of 92%, stir to completely dissolve the licorice flavonoids, then slowly add 200g of β-cyclodextrin, and stir at room temperature for 1 hour. Make cyclodextrin fully include licorice flavonoids. Then dry it at 70-80°C under the condition of vacuum -0.07Pa, steam until the clathrate has no ethanol smell, and obtain a yellow, dry clathrate. Dissolve the inclusion compound in 750 g of deionized water and stir well for about 1 hour, filter, collect the filtrate, and distill to a water-soluble flavonoid with a concentration of licorice flavonoids of 7% and a light yellow color.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com