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Process for vacuum melting and spurting of titanium-cobalt-manganese-scandium alloy

A vacuum smelting and alloying technology, which is applied in the field of vacuum smelting and sputtering titanium-cobalt-manganese-scandium alloys, can solve the problems of abnormal smelting process, high melting point, high cost, etc., achieve good thermodynamic stability, reduce manufacturing costs, and equipment low cost effect

Inactive Publication Date: 2011-06-01
张舒然
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Under the current metallurgical technology conditions, titanium-cobalt-manganese-scandium alloy series materials are easy to oxidize and volatilize because of their high melting point. The alloy is melted in a vacuum in a conventional clay graphite crucible. The alloy liquid will be polluted by the crucible material and volatilized by low melting point elements As a result, the smelting process cannot be carried out normally, nor can it fail to meet the quality standards required by the alloy.
At present, most foreign countries use advanced vacuum plasma melting technology to smelt such alloys, which is expensive and expensive.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Use a thermodynamically stable pure graphite crucible to melt titanium-cobalt-manganese-scandium alloy under positive pressure nitrogen atmosphere. Industrial pure scandium is used as raw material, and the weight percentage in the alloy is titanium: cobalt: manganese: scandium = 46: 41: 8: 5; the furnace is loaded in the following order: titanium and cobalt are loaded into a pure graphite crucible, manganese and scandium are loaded into a hopper , added at the later stage of smelting;) Melting preparation: first vacuumize the furnace body, when the vacuum in the furnace is equal to 0.65Pa, fill the furnace with nitrogen, and increase the pressure to 0.8Mpa; alloy melting: power transmission, melting titanium and cobalt, combined After melting, flip the hopper and add manganese and scandium; casting of alloy: After all the alloy raw materials are melted, they are refined and placed, and when the temperature reaches 1350-1390°C, the alloy liquid is poured to cast titanium,...

Embodiment 2

[0025] Use a thermodynamically stable pure graphite crucible to melt titanium-cobalt-manganese-scandium alloy under positive pressure nitrogen atmosphere. Industrial pure scandium is used as raw material, and the weight percentage in the alloy is titanium: cobalt: manganese: scandium = 43:35:15:7; the furnace is loaded in the following order: titanium and cobalt are loaded into a pure graphite crucible, manganese and scandium are loaded into a hopper , added at the later stage of smelting; smelting preparation: first vacuumize the furnace body, when the vacuum in the furnace is equal to 0.55Pa, fill the furnace with nitrogen, and increase the pressure to 0.8Mpa; alloy melting: power transmission, melting titanium and cobalt, melting the joint Finally, turn over the hopper, add manganese and scandium; alloy pouring: after melting all the alloy raw materials, refine and set aside, when the temperature reaches between 1250 and 1290°C, pour the alloy liquid to cast titanium cobalt ...

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PUM

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Abstract

The invention relates to a process for vacuum spurting and melting of a titanium-cobalt-manganese-scandium alloy, which is characterized by comprising the following step: by using a thermodynamically-stable pure graphite crucible, melting a titanium-cobalt-manganese-scandium active alloy in a positive-pressure atmosphere. Compared with other vacuum metallurgy technologies, such as electron beam and plasma arc melting, vacuum consumable melting and the like, the vacuum spurting and melting technology provided by the invention has the advantages of low equipment cost and simple process, is convenient to operate, and greatly lowers the alloy manufacturing cost, thereby realizing the practical application of the titanium-cobalt-manganese-scandium alloys. Besides, the process for vacuum melting of a titanium-cobalt-manganese-scandium alloy can prevent the crucible material from reacting with active elements in the alloy in the melting process, lowers the oxygen content in the alloy, reduces the volatilization of low-melting point elements and improves the purity of the melted alloy.

Description

technical field [0001] The invention relates to vacuum metallurgy technology, in particular to a process for vacuum melting and sputtering titanium-cobalt-manganese-scandium alloy. Background technique [0002] Under the current metallurgical technology conditions, titanium-cobalt-manganese-scandium alloy series materials are easy to oxidize and volatilize because of their high melting point. The alloy is melted in a vacuum in a conventional clay graphite crucible. The alloy liquid will be polluted by the crucible material and volatilized by low melting point elements As a result, the smelting process cannot be carried out normally, and the quality standard required by the alloy cannot be reached. At present, most foreign countries use advanced vacuum plasma melting technology to smelt such alloys, which is expensive and expensive. Contents of the invention [0003] The purpose of the present invention is to provide a process for vacuum smelting titanium-cobalt-manganese-...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/02B22D21/06
Inventor 张舒然
Owner 张舒然
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