Thermal expansion water-blocking filling paste for optical cables and preparation method thereof
A technology of water blocking filling and thermal expansion, which is applied in the direction of fiber mechanical structure, etc., can solve the problems of destroying the structural material of the optical cable, cannot guarantee, affect the safety of optical cable communication operation, etc., and achieve the effect of improving quality, good compression resistance, and high expansion ratio
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Embodiment 1
[0026] Add 40 grams of high-molecular polymer synthetic rubber to 891 grams of hydrogenated white oil, heat and stir for 3 to 5 hours, when the temperature rises to 200 ° C, add 5 grams of high-temperature antioxidant, fully stir for 0.5 to 1 hour, and then Cool down to 20 ℃ ~ 60 ℃, add 60 grams of fumed silica at high speed, the speed is 1000 ~ 2800 rpm, stir well for 0.5 ~ 1 hour, add 3 grams of dispersant, and then disperse at high speed, the speed is 1000 ~ 2800 rpm, to obtain a semi-fluid compound, after grinding and homogenizing, add 1 gram of heat-expandable microsphere foaming agent, fully return the material and stir for 0.5 to 1 hour, then vacuum degas, and finally obtain a milky white paste compound product.
[0027] Among the above raw materials, the high-temperature antioxidant is selected from Ciba Specialty Chemicals (China) Co., Ltd., model L101, and the dispersant is selected from polyester grade ethylene glycol produced by Zhejiang Nice Group Co., Ltd.
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Embodiment 2
[0030] Add 50 grams of high-molecular polymer synthetic rubber to 886.5 grams of naphthenic rubber oil, heat and stir for 3 to 5 hours, when the temperature rises to 200 ° C, add 5 grams of high-temperature antioxidant, and fully stir for 0.5 to 1 hour, Then cool down to 20 ℃ ~ 60 ℃, add 55 grams of bentonite at high speed dispersion, the speed is 1000 ~ 2800 rpm, after stirring for 0.5 ~ 1 hour, add 2 grams of dispersant, and then disperse at high speed, the speed is 1000 ~ 2800 rpm / min, to obtain a semi-fluid compound, after grinding and homogenizing, add 1.5 grams of heat-expandable microsphere foaming agent, fully return the material and stir for 0.5 to 1 hour, then vacuum degassing, and finally obtain a milky white paste compound product .
[0031] This product: flash point > 200°C, dropping point > 200°C, penetration 365 1 / 10mm, oil separation 0%, acid value 0.25mgKOH / g, oxidation induction period (190°C) ≥ 60min, expansion temperature start temperature 130-140°C, fina...
Embodiment 3
[0033] Add 45 grams of high-molecular polymer synthetic rubber to 880 grams of paraffin-based rubber oil, heat and stir for 3 to 5 hours, when the temperature rises to 200 ° C, add 5 grams of high-temperature antioxidant, stir thoroughly for 0.5 to 1 hour, and then Cool down to 20°C-60°C, add 65 grams of fumed silica at a high speed at a speed of 1000 to 2800 rpm, stir well for 0.5 to 1 hour, add 3 grams of a dispersant, and then disperse at a high speed at a speed of 1000 to 1 2800 rpm to get a semi-fluid compound, after grinding and homogenizing, add 2 grams of heat-expandable microsphere foaming agent, fully return the material and stir for 0.5-1 hour, then vacuum degas, and finally get a milky white paste compound product.
[0034] This product: flash point > 200°C, dropping point > 200°C, penetration 355 1 / 10mm, oil separation 0%, acid value 0.26mgKOH / g, oxidation induction period (190°C) ≥ 60min, expansion temperature start temperature 130-140°C, final temperature 165-1...
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