Resin, pigment dispersion liquid, coloring curable composition, color filter produced by using composition, and method for producing color filter
一种固化性组合物、制造方法的技术,应用在滤光片、有机染料、图纹面的照相制版工艺等方向,能够解决图案形成变困难、分散性·分散稳定性·显影性变差等问题,达到分散性·分散稳定性优异、色特性良好、色纯度高的效果
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[0442] Hereinafter, although an Example demonstrates this invention in more detail, this invention is not limited to this.
[0443] It should be noted that, in the examples, the acid value and the amine value use the potential difference method (solvent tetrahydrofuran / water=100 / 10 (volume ratio), titration solution 0.01N sodium hydroxide aqueous solution (acid value) 0.01N hydrochloric acid ( Amine value)) to decide. However, in Example 18 and Example 29, instead of the 0.01N aqueous sodium hydroxide solution, the titration was performed with a 0.01N sodium methoxide dioxane solution system.
Synthetic example 1
[0444] (Synthesis example 1) Synthesis of polyester (i-1)
[0445] 6.4 g of n-octanoic acid, 200 g of ε-caprolactone, and 5 g of tetrabutoxytitanium (IV) were mixed, heated at 160° C. for 8 hours, and then cooled to room temperature to obtain polyester (i-1).
[0446] The diagram is shown below.
[0447] [chem 36]
[0448]
Synthetic example 2~10
[0450] Polyesters (i-2) to (i-10) were obtained in the same manner as in Synthesis Example 1 except that the amount of preparation was described in Table 1. The number-average molecular weight and weight-average molecular weight of the resins obtained in these synthesis examples were measured by the GPC method already described. The results are shown in Table 1 below. In addition, the number of lactone repeating units calculated from the raw material charging ratio is also shown in Table 1 below.
[0451] 【Table 1】
[0452]
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