Preparation method of composite sol and method for producing solar battery packaging glass by using same
A technology for solar cells and encapsulation glass, which is applied in the preparation of composite sol and in the field of manufacturing encapsulation glass for solar cells, can solve the problems of poor film-forming properties, hardness, resistance to salt spray, complicated operation, and inability to achieve
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Embodiment 1
[0037] A method for preparing a composite sol for solar cell encapsulation glass coated with an anti-reflection film of the present embodiment comprises the following steps:
[0038] Step 1: Mix silicon alkoxide, water, basic catalyst and alcoholic organic solvent according to the volume ratio of 1-100:0.1-10:0.01-1:3-300 to form mixed solution A. The silicon alkoxide is mixed under alkaline conditions according to the volume ratio of silicon alkoxide, water, basic catalyst and alcohol organic solvent respectively 1-100:0.1-10:0.01-1:3-300, and the formed The stability of mixed solution A is better.
[0039] Step 2, adjusting the pH value of the mixed solution A in step 1 to 8-10.
[0040] Step 3: Add an inhibitor and a dispersant to the mixed solution A after adjusting the pH value in Step 2, mix and stir at room temperature for 1h-10h, seal and leave to age for 1d-10d to obtain the first sol. Adding inhibitors and dispersants can control the reaction process, so that the p...
Embodiment 2
[0053] A method for preparing a composite sol for solar cell encapsulation glass coated with an anti-reflection film of the present embodiment comprises the following steps:
[0054] Step 1: Mix methyl orthosilicate, water, ammonia water and anhydrous methanol according to the volume ratio of 75-90:1.4-8.8:0.05-0.09:110-250 to form a mixed solution A. Firstly, methyl orthosilicate is used to prepare a sol with better stability under alkaline conditions to ensure its low refractive index.
[0055] Step 2, adjusting the pH value of the mixed solution A in step 1 to 8.5-9.5.
[0056] Step 3: Add polyvinyl alcohol and glycerol to the mixed solution A after adjusting the pH value in Step 2, mix and stir at room temperature for 5h-8h, seal and leave to age for 6d-8d to obtain the first sol.
[0057] Step 4, changing the reaction conditions, adding glacial acetic acid, acetylacetone and diethanolamine to the first sol obtained in Step 3 to form a mixed solution B.
[0058] Step fiv...
Embodiment 3
[0062] A method for preparing a composite sol for solar cell encapsulation glass coated with an anti-reflection film of the present embodiment comprises the following steps:
[0063] Step 1: Mix silicon alkoxide, water, triethanolamine and isopropanol according to the volume ratio of 20-75:0.2-1.4:0.02-0.07:3-110 to form a mixed solution A.
[0064] Step 2, adjusting the pH value of the mixed solution A in step 1 to 8.1-9.4.
[0065] Step 3: Add polyethylene glycol and CMC to the mixed solution A after pH adjustment in Step 2, mix and stir at room temperature for 2h-6h, seal and leave to age for 1d-3d to obtain the first sol.
[0066] Step 4, changing the reaction conditions, adding sulfuric acid, acetylacetone and diethanolamine to the first sol obtained in Step 3 to form a mixed solution B.
[0067] Step five, adjusting the pH value of the mixed solution B in step four to 3-4.
[0068] Step 6: Add a certain amount of zirconium oxychloride as a zirconium source to the mixed...
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