Preparation method of graphene inorganic nanocomposite
A composite material and inorganic nanotechnology, applied in the field of functional material chemistry and nanomaterials, can solve problems such as difficult to achieve large-scale preparation, high reaction conditions, and multiple processing steps, and achieve short reaction time, simple process flow, and high surface area Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0021] 1. Preparation of graphite oxide. Take 1.5g of flake graphite powder, 1.5g of sodium nitrate, and 70ml of concentrated sulfuric acid, add them to the there-necked flask in turn, stir evenly under ice bath conditions, slowly add 9g of potassium permanganate, then warm up to room temperature for 2 hours, then add 100ml of distilled water, Then the temperature was raised to 90° C. for 1 h. Then add 300ml of distilled water and 10ml of 30% H to the reaction system 2 o 2 . Then the above solution was centrifuged several times, washed several times with dilute hydrochloric acid, distilled water and absolute ethanol successively, and the product was dried at 80°C to obtain graphite oxide.
[0022] 2. Preparation of graphene. Take 10mg of graphite oxide and disperse it in 50ml of distilled water, and ultrasonically strip it to obtain an aqueous solution of graphene oxide, add 10ml of 30% hydration trap, react at room temperature for 24h, then raise the temperature to 100°C ...
Embodiment 2
[0025] 1, the preparation of graphite oxide and graphene is identical with embodiment 1.
[0026] 2. Weigh the zinc sulfate solid and dissolve it in distilled water to form a 0.2mol / L solution. Take 100ml of the solution, then add 15mg of graphene, ultrasonicate for 30 minutes, and slowly add 0.3mol / L of The oxalic acid solution was used as a precipitating agent until no new precipitation was produced. The mixed solution was centrifuged at high speed and washed several times with distilled water. The obtained product was first dried at 80°C for 10 hours, and then heat-treated at 500°C for 2 hours to obtain graphene / ZnO inorganic nanocomposites. .
Embodiment 3
[0028] 1, the preparation of graphite oxide and graphene is identical with embodiment 1.
[0029] 2. Weigh cerium nitrate solid and dissolve it in distilled water to form a 0.3mol / L solution. Take 150ml of the solution, then add 10mg of graphene, ultrasonicate for 30 minutes, and slowly add 0.3mol / L of The oxalic acid solution was used as a precipitant until no new precipitation was produced. The mixture was centrifuged at high speed and washed several times with distilled water. The obtained product was first dried at 80°C for 10h, and then heat-treated at 600°C for 2h to obtain graphene / CeO 2 Inorganic Nanocomposites.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com