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Method for preparing soluble plantain seed dietary fiber and application thereof

A dietary fiber and soluble technology, which is applied in the field of preparation of psyllium soluble dietary fiber, can solve the problems of psyllium soluble dietary fiber, such as dark color, low purity, and poor water resolubility, and achieve high purity, simple process operation, Good water resolubility effect

Inactive Publication Date: 2012-11-28
NANCHANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Existing open technology Chinese patent at present: publication number is CN101269124A " a kind of plantago polysaccharide oral preparation, preparation method and application " patent document adopts microwave extraction, and the amount of water added is 10-15 times of plantago weight, then concentrates, Then add 2 times the weight of absolute ethanol for alcohol precipitation. This method directly uses a large amount of absolute ethanol for precipitation, making the ethanol mass concentration as high as 66.7%. The psyllium soluble dietary fiber will wrap a large amount of water-soluble Sexual impurities, the prepared psyllium soluble dietary fiber has a darker color, lower purity, and poor water resolubility

Method used

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  • Method for preparing soluble plantain seed dietary fiber and application thereof
  • Method for preparing soluble plantain seed dietary fiber and application thereof
  • Method for preparing soluble plantain seed dietary fiber and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Weigh 490g of sieved and cleaned Plantago Seeds, add 9.8L of water, extract for 3 hours at 100°C, twice, filter while hot, combine the filtrate, concentrate to a specific gravity of 1.07, add chlorination at 3% of the weight of the concentrate Sodium, stir to dissolve it completely, let it cool, then add ethanol precipitation under stirring to make the ethanol mass concentration reach 30%, let stand alcohol precipitation, centrifugal separation, wash with a small amount of 85% ethanol, vacuum dry, pulverize and pass through 120 mesh sieve. 39.1 g of psyllium soluble dietary fiber raw material powder was obtained, the yield was 7.68%, and the purity was 88.1%.

Embodiment 2

[0019] Weigh 650g of sieved and cleaned plantago seeds, add 6.5L of water, extract for 2.5h at 100℃, twice, filter while hot, combine the filtrate, concentrate to a specific gravity of 1.04, add chlorine at 7% of the weight of the concentrate Dissolve ammonium, stir to completely dissolve, let cool, then add ethanol under stirring for precipitation, and make the ethanol mass concentration reach 55%, stand still for alcohol precipitation, centrifugal separation, wash with a small amount of 85% ethanol, reconstitute with water, and get the car Pre-child soluble dietary fiber raw material solution.

Embodiment 3

[0021] Weigh 470g of sieved and cleaned Plantago seeds, add 2.35L of water, extract for 1 hour at 80℃, filter while hot, combine the filtrate, concentrate to a specific gravity of 1.02, add calcium chloride at 1.25% of the weight of the concentrate , Stir to make it completely dissolved, let it cool, then add ethanol under stirring to precipitate, and make the ethanol mass concentration reach 36%, let stand alcohol precipitation, centrifuge, wash the precipitate with a small amount of 85% ethanol, freeze-dry, pulverize through 120 mesh After sieving, 21.1 g of psyllium soluble dietary fiber raw material powder was obtained, the yield was 4.5%, and the purity was 89.3%.

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Abstract

The invention provides a method for preparing soluble plantain seed dietary fiber and application thereof. The method is characterized by comprising the following steps: (1) subjecting plantain seed to sieving, impurity removal and hot-water extraction; (2) combining and concentrating the water extract until the specific gravity thereof is 1.02 to 1.10, adding soluble salts with the concentrationthereof being 0.3% to 7%, further adding ethanol precipitation until the concentration thereof reaches 30% to 55%, and subjecting the precipitation to centrifugal separation and ethanol (85%) rinsing; and (3) drying and grinding the precipitation in step (2) to obtain the soluble plantain seed dietary fiber powder or the plantain seed dietary fiber solution. The invention has the following advantages: 1, the method is capable of removing most soluble impurities, so the obtained soluble plantain seed dietary fiber has lighter color, higher purity and better water-solubility; compared with the ethanol precipitation with the mass concentration thereof being adjusted to 66.7%, the ethanol for ethanol precipitation can be saved by 55% under the optimal conditions; and the added salts or acids for ethanol precipitation are food additives, so the product subjected to ethanol precipitation and rinsing is almost residue-free; 2, the prepared soluble plantain seed dietary fiber is applicable tofood, health-care food or drug achieving the effects of moistening the intestine and relaxing the bowel; and 3, the process has the advantages of simple operation, water-saving, energy-saving and environment-friendly application, so the method is applicable to industrialized production.

Description

Technical field [0001] The invention relates to a preparation method and use of dietary fiber, in particular to a preparation method and use of psyllium soluble dietary fiber. Background technique [0002] Dietary fiber refers to the polymer of carbohydrates that cannot be digested and absorbed in the small intestine. Its degree of polymerization (DP) is not less than 3, and has many important physiological functions for human health. It is recognized by modern medicine and nutrition as the traditional six major The "seventh nutrient", which is a juxtaposition of nutrients, is classified into soluble dietary fiber and insoluble dietary fiber according to its solubility in hot water. The essence of the soluble dietary fiber of Psyllium is polysaccharides. It is a nutritious food with special physiological and health care functions. It can supplement the dietary fiber needed by the human body. After entering the human digestive system, it produces special physiological metabolic fu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23L1/28A23L1/308A61K36/68A61P1/10A61P3/06A23L33/10A23L33/105A23L33/21
Inventor 田颖刚谢明勇
Owner NANCHANG UNIV
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