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Molten metal oxidation-resistant chelating reducer

A technology of melting metal and oxidizing chelate, applied in the direction of metal material coating process, etc., can solve the problems of carcinogens, low reduction rate, high price, etc., and achieve the effect of no carcinogens, high reduction efficiency, and quality improvement.

Inactive Publication Date: 2011-01-26
薛永春
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to solve the above problems, reducing powder is often used in the prior art. Due to the raw material composition of molten metal reducing powder, this type of reducing powder has the following defects: poisonous, low reduction rate; because there is strong acid in the ingredients, most of them are strong acids Strong alkali is corrosive to the machine, and the smoke is large
In addition, there is also a type of molten metal reducing agent. This type of reducing agent is also toxic. It contains carcinogens and is irritating to the human body. The smoke has a strong smell and is corrosive to the machine. The residue is gelatinous and difficult to clean. Defects that do not meet environmental protection standards and are very expensive
In the prior art, there is also the use of a molten metal reduction machine. This solution has the following problems: the quality of the molten metal itself after reduction is poor, and it consumes electricity, manpower management and space placement.
In addition, the chelating effect of the current antioxidant chelating reducing agent is not obvious, so that the metal content of the recycled tin sludge is relatively high, so that the oxide content in the tin water increases, and the processed product will produce empty welding, which will affect the quality of the processed product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] When in the technology of molten metal, sign to the situation of lead-free tin with high silver content, the parts by weight of various compositions of the present invention are as follows: polyoxyethylene ether nonylphenol phosphate ester 55 parts, ammonium dihydrogen phosphate 30 parts, 10 parts of ammonium hydroxysuccinate. The production process of the present invention comprises the following steps: first, take out the polyoxyethylene ether nonylphenol phosphate, ammonium dihydrogen phosphate and ammonium hydroxysuccinate in the above-mentioned weight ratio as required. In this embodiment, the specific weight is 55 kg of polyoxyethylene ether nonylphenol phosphate, 30 kg of ammonium dihydrogen phosphate, and 10 kg of ammonium hydroxysuccinate; first heat polyoxyethylene ether nonylphenol phosphate to 180°C, and then add hydroxysuccinate ammonium Stir slowly until it is completely dissolved, then cool; after cooling, slowly add ammonium dihydrogen phosphate and stir...

Embodiment 2

[0029] Embodiment 2: This embodiment is still the case of lead-free tin with high silver content, and its optimized process formula is: 60 parts of polyoxyethylene ether nonylphenol phosphate, 35 parts of ammonium dihydrogen phosphate, 5 parts of ammonium hydroxysuccinate share. In this embodiment, the specific weight ratio is: 60 kg of polyoxyethylene ether nonylphenol phosphate, 35 kg of ammonium dihydrogen phosphate, and 5 kg of ammonium hydroxysuccinate.

[0030] Other parts of this embodiment are identical to Embodiment 1.

Embodiment 3

[0031] Embodiment 3: This embodiment is still another preferred process formula for the situation of high silver content lead-free tin: 65 parts of polyoxyethylene ether nonylphenol phosphate, 27 parts of ammonium dihydrogen phosphate, ammonium hydroxysuccinate 2 servings. In this embodiment, the specific weight ratio is: 65 kg of polyoxyethylene ether nonylphenol phosphate, 27 kg of ammonium dihydrogen phosphate, and 2 kg of ammonium hydroxysuccinate.

[0032] Other parts of this embodiment are identical to Embodiment 1.

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PUM

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Abstract

The invention belongs to a molten metal oxidation-resistant chelating reducer used for manufacturing electronic products. The molten metal oxidation-resistant chelating reducer comprises polyoxyethylene nonyl phenyl ether phosphate, ammonium biphosphate and hydroxyl ammonium succinate, and comprises the following parts by weight: 55-95 parts of the polyoxyethylene nonyl phenyl ether phosphate, 10-40 parts of the ammonium biphosphate and 2-10 parts of the hydroxyl ammonium succinate. The molten metal oxidation-resistant chelating reducer has the beneficial effects of high reduction efficiency,being nontoxic, no carcinogen, little smoke, and no corrosion to machines due to neutral pH value. The reducer also can help remove excess metals and oxidation impurities released on tin surface froma tin furnace to play the role of purification; and the reducer can react with a carbonizing soldering flux in a high-temperature furnace, thus further improving reduction effect and releasing metallic elements. The reducer has the advantages of being capable of further improving electronic industry quality, saving energy and reducing consumption, and being safe, efficient and convenient.

Description

【Technical field】 [0001] The invention relates to a molten metal anti-oxidation chelating reducing agent, which belongs to a chemical chelating reducing agent, in particular to a molten metal anti-oxidizing chelating reducing agent used in the manufacture of electronic products. 【Background technique】 [0002] Molten metals are often used in the manufacture of electronic products. Molten metals (or alloys) will be oxidized when they encounter air, melted and oxidized in a high-temperature furnace, and continue to circulate in the furnace, the oxidation speed will be accelerated, and the amount of oxidized metal will increase. It will increase, and the oxide will contain carbonized flux that contains a lot of tin, and it will accumulate and float on the tin surface to affect the flow of tin and the quality of tin on the surface, so it can only be salvaged. After the tin slag is salvaged, the height of the tin surface will be reduced, so tin strips should be added frequently. ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C22/07
Inventor 何光宁
Owner 薛永春
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