Method for manufacturing high wet modulus fiber
A technology of high wet modulus fiber and manufacturing method, applied in wet spinning, fiber processing, textile and papermaking, etc., can solve the problems of harsh raw material requirements, high hemicellulose, increase the cost of raw materials for fiber production, etc., and achieve high strength. , bright dyeing effect
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Embodiment 1
[0037] Using a cellulose content (the content refers to the weight percentage, the same below) of 92% wood cellulose pulp is immersed and alkalized by 230g / l NaOH solution once, the concentration of the porridge is 4.5%, and the immersion temperature is At 50°C, add 0.1% of the viscose auxiliary agent relative to the methyl cellulose content-fatty alcohol ether (code EBZ) during dipping, and the first dipping time is 1.5 hours. After squeezing and crushing, it is dipped and alkalized by 160g / l NaOH solution twice. The concentration of the second dipping porridge is 4.0%, the second dipping temperature is 42℃, and the second dipping time is 1 hour. Cellulose dissolves, and its content is less than 20g / l. After squeezing and pulverizing again, an alkali cellulose with a squeezing ratio of 2.8 and a pulverization degree of 120 g / l was obtained. Alkaline cellulose is aged at 30°C for 4 hours to produce alkali cellulose with a cupramide viscosity of 70 mps. Combine 7500kg of alkali cel...
Embodiment 2
[0039] Wood cellulose pulp with a cellulose content of 89% and cotton pulp with a cellulose content of 94%, each accounting for 50% of the total weight of the raw materials, are mixed, and then immersed and alkalized by a 240g / L NaOH solution. The concentration of porridge is 4.8%, the immersion temperature is 52°C, the immersion time is 1 hour, and the viscose auxiliary agent-fatty alcohol ether (code EBZ), which is 0.1% relative to the methyl cellulose content, is added. After squeezing, it is immersed and alkalized by 170g / l NaOH solution twice. The concentration of the porridge is 4.5%, the temperature of the second immersion is 48℃, and the time of the second immersion is 1.5 hours, so that the half fiber in the lye can be impregnated. The dissolution of vegetarian, its content is less than 25g / l. After squeezing and pulverizing again, alkali cellulose with a squeezing ratio of 3.0 is obtained. The alkali cellulose is aged for 5 hours at 25°C to produce alkali cellulose with ...
Embodiment 3
[0041] The cotton pulp with a cellulose content of 94.5% was immersed and alkalized by a 235g / l NaOH solution. The concentration of the porridge was 3.8%, the immersion temperature was 52℃, and the amount of para-methyl cellulose was 0.2. % Of viscose additives-fatty alcohol ether (code EBZ). The immersion time is 2.5 hours to dissolve the hemicellulose in the immersion alkali solution, and its content is less than 30g / l. After squeezing and pulverizing, alkali cellulose with a squeezing ratio of 3.2 is obtained. Alkali cellulose is aged for 2.5 hours at 35°C to produce alkali cellulose with a copper ammonia viscosity of 80 mps. Combine 8000kg of alkali cellulose with 840 liters of CS 2 The yellowing reaction takes 55 minutes to generate cellulose xanthate. After the yellowing is completed, add 48g / l of NaOH dilute lye to dissolve at 8°C. During the dissolution of cellulose xanthate, add 2.0% relative to the weight of methyl cellulose. The viscose denaturant-the alkylene oxide add...
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