Emission early-warning monitoring method for organic arsenic feed additive in water environment system
A feed additive, early warning monitoring technology, applied in the preparation of test samples, color/spectral characteristic measurement, etc., can solve the problems of high reagent cost and harsh experimental equipment conditions.
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example 1
[0025] (1) culture medium preparation;
[0026] Weigh 10g of peptone and 2g of glucose, dissolve them in 1000mL of deionized water, stir evenly, distribute them in 150mL Erlenmeyer flasks (each bottle has 80mL medium), sterilize in an autoclave at 121°C for 20-30min, and then statically Bring to room temperature and store in a refrigerator at 4°C.
[0027] (2) Preparation of arsanic acid organic arsenic feed additive standard sample solution;
[0028] Weigh 28.98 mg of arsanic acid standard sample and 0.05 g of sodium hydroxide, dissolve them in deionized water, and finally make up to volume in a 100 mL volumetric flask. ready for dilution
[0029] (3) Collect actual water samples and extract possible organic arsenic feed additive compounds;
[0030] Take 5.0ml of the actual water sample and filter it through a 0.45μm filter membrane. Finally, place 0.01g of nano-ferromagnetic adsorbent in the corresponding actual water sample, adjust its pH value to 4.5 (using acetic acid...
example 2
[0041] (1) Tetrahymena medium preparation;
[0042] Weigh 10g of peptone, 2g of glucose, and 1g of yeast extract powder, dissolve them in 1000mL of deionized water, stir well, distribute them in 150mL Erlenmeyer flasks (80mL of medium in each bottle), and sterilize them in an autoclave at 121°C After 20-30min, let stand to room temperature, and store in refrigerator at 4°C.
[0043] (2) Preparation of arsanic acid organic arsenic feed additive standard sample solution;
[0044] Weigh 28.98 mg of arsanic acid standard sample and 0.05 g of sodium hydroxide, dissolve in deionized water, and finally make up to volume in a 100 mL volumetric flask. The total arsenic concentration in the corresponding standard solution is 100 μg / ml, and store in a refrigerator for future use Use diluted.
[0045] (3) Collect actual water samples and extract possible organic arsenic feed additive compounds;
[0046] Take 5.0ml of the actual water sample and filter it through a 0.45μm filter membran...
example 3
[0057] (1) Tetrahymena medium preparation;
[0058] Weigh 10g of peptone and 2g of glucose, dissolve them in 1000mL of deionized water, stir evenly, distribute them in 150mL Erlenmeyer flasks (each bottle has 80mL medium), sterilize in an autoclave at 121°C for 20-30min, and then statically Bring to room temperature and store in a refrigerator at 4°C.
[0059] (2) Roxars arsenic organic arsenic feed additive standard sample solution preparation;
[0060] Weigh 35.82mg of roxarsarsenic standard sample, 0.05g of sodium hydroxide, dissolve in deionized water, and finally make up to volume in a 100mL volumetric flask. Prepare for dilution.
[0061] (3) Collect actual water samples and extract possible organic arsenic feed additive compounds;
[0062] Take 5.0ml of the actual water sample and filter it through a 0.45μm filter membrane. Finally, place 0.01g of nano-ferromagnetic adsorbent in the corresponding actual water sample, adjust its pH value to 4.5 (using acetic acid-sod...
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