Process for preparing zinc oxide nano film
A zinc oxide nanometer and thin film technology, applied in nanostructure manufacturing, zinc oxide/zinc hydroxide, nanotechnology, etc., can solve the problems of high cost, high energy consumption, complex equipment and process, etc.
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[0009] In conjunction with the accompanying drawings, the preparation method of the zinc oxide nano film of the present invention comprises the following steps: first, in concentrated hydrochloric acid, add butyl zincate, stir, the solution presents a transparent and clear shape, prepare a precursor solution, and spread it on the culture In the container; secondly, add the surfactant into the water, heat and stir to obtain the template solution; then, after the template solution is cooled, pour it evenly into the culture container, transfer it to the artificial intelligence climate box, and let it stand for self-assembly to obtain ZnO nanofilms. Among them, the surfactant is sodium dodecylsulfonate SDS1, sodium dodecylsulfate SDS2, sodium dodecylbenzenesulfonate DBS-Na, 1-sodium naphthalenesulfonate 1-SNS or 2-naphthalenesulfonic acid Sodium 2-SNS. Protein gelatin can be added to the surfactant as a film-forming aid. The mass ratio of surfactant to gelatin is 1:1-2:1. The m...
Embodiment 1
[0012] Step 1, dissolving 0.84g of butyl zincate in 0.64g of 37% concentrated hydrochloric acid HCl, and magnetic stirring for 10min to obtain a clear precursor solution;
[0013] Step 2, spreading the above solution in a plastic petri dish;
[0014] Step 3, dissolve 0.15 g of the surfactant sodium dodecylsulfonate (SDS) in 18.4 ml of deionized H 2 O, heated to 40°C with magnetic stirring for 15 minutes to obtain a uniformly mixed templating agent, and cooled at room temperature;
[0015] Step 4, when the temperature of the above-mentioned cooling solution is slightly higher than normal temperature (about 25°C), pour it evenly into the petri dish;
[0016] Step 5, transfer the petri dish to a thermostatic chamber (keep the film growth temperature at 21° C.), and let it stand still. After about 12 hours, the self-assembly process is completed to obtain a zinc oxide nano film.
[0017] The present invention uses the obtained zinc oxide nano film as the starting material, heats...
Embodiment 2
[0019] Step 1, with embodiment 1;
[0020] Step 2, with embodiment 1;
[0021] Step 3, mix 0.15g of surfactant sodium dodecyl sulfate (SDS2) and 0.15g of gelatin (G) and dissolve in 18.4ml of deionized H 2 O, heated to 30°C with magnetic stirring for 18 minutes to obtain a uniformly mixed template solution, and cooled at room temperature;
[0022] Step 4, with embodiment 1;
[0023] Step 5, with embodiment 1;
[0024] Step 6 is the same as in Example 1.
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