Method for synthesizing triptorelin from solid phase polypeptide
A solid-phase peptide synthesis and peptide cleavage technology, which is applied in the field of triptorelin preparation, can solve the problems of polluting the environment, restricting the large-scale production and use of triptorelin acetate, and low yield of peptides.
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Embodiment 1
[0103] The list of raw materials adopted in the embodiment and the foregoing process is as follows:
[0104] no
product name
manufacturer
1
resin
Tianjin Hecheng Technology Co., Ltd.
2
Fmoc-Gly-OH
Suzhou Tianma Pharmaceutical Group
3
Fmoc-Pro-OH
Suzhou Tianma Pharmaceutical Group
4
Fmoc-Arg(Pbf)-OH
Suzhou Tianma Pharmaceutical Group
5
Fmoc-Leu-OH
Suzhou Tianma Pharmaceutical Group
6
Fmoc-D-Trp-OH
Suzhou Tianma Pharmaceutical Group
7
Fmoc-D-Trp(Boc)-OH
Suzhou Tianma Pharmaceutical Group
8
Fmoc-Tyr(tBu)-OH
Suzhou Tianma Pharmaceutical Group
9
Fmoc-Ser(tBu)-OH
Suzhou Tianma Pharmaceutical Group
10
Fmoc-Trp-OH
Suzhou Tianma Pharmaceutical Group
11
Fmoc-Trp(Boc)-OH
Suzhou Tianma Pharmaceutical Group
12
Fmoc-His(Trt)-OH
Suzhou Tianma Pharmaceutical Group
13 ...
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