Process for preparing rubber accelerator TBBS
A technology of rubber accelerator and production method, applied in organic chemistry and other directions, can solve the problems of large distillation load, large amount of waste water and high COD, and achieve the effects of reducing waste water discharge, saving energy and improving M conversion rate
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Embodiment 1
[0015] The production method of rubber accelerator TBBS of the present invention is made up of following steps successively:
[0016] a, oxidation reaction: with 500 kilograms of raw materials M, 600 kilograms of tert-butylamine and 0.5 kilogram of carbonic acid, add 5500 kilograms of water and stir evenly, keep the temperature in the oxidation kettle at 30-50 ℃, add 436 kilograms of hydrogen peroxide solution with a mass content of 28% (hydrogen peroxide molecular weight: 34.01) was oxidized, and the oxidation time was 7 hours;
[0017] b. The oxidized material is distilled to recover tert-butylamine: adopt the vacuum distillation method, the vacuum degree is 0.03-0.09MPa, the temperature at the top of the tower is 20-25°C, the temperature at the bottom of the tower is 20-25°C, and the distillation time is 5 hours;
[0018] c. The remaining material after distillation is placed in a centrifuge and washed with water in a conventional manner until pH = 7 to obtain a finished pr...
Embodiment 2
[0021] The production method of rubber accelerator TBBS of the present invention is made up of following steps successively:
[0022] a, oxidation reaction: with 500 kilograms of raw materials M, 2000 kilograms of tert-butylamine and 50 kilograms of acetic acid, add 7500 kilograms of water and stir evenly, keep the temperature in the oxidation kettle at 30-50 ° C, add 654 kilograms of hydrogen peroxide solution with a mass content of 28% (hydrogen peroxide molecular weight: 34.01) is oxidized, and the oxidation time is 3 hours;
[0023] b. The oxidized material is distilled to recover tert-butylamine: adopt the vacuum distillation method, the vacuum degree is 0.03-0.09MPa, the temperature at the top of the tower is 60-65°C, the temperature at the bottom of the tower is 75-80°C, and the distillation time is 2 hours;
[0024] c. The remaining material after distillation is washed with water in a centrifuge until pH = 7 to obtain the finished product of TBBS.
[0025] All the ot...
Embodiment 3
[0027] The production method of rubber accelerator TBBS of the present invention is made up of following steps successively:
[0028] a. Oxidation reaction: Add 500 kg of raw material M, 1300 kg of tert-butylamine and 25 kg of oxalic acid, add 6500 kg of water and stir evenly, keep the temperature in the oxidation kettle at 30-50 ° C, add 550 kg of hydrogen peroxide solution with a mass content of 28% for oxidation , the oxidation time is 5 hours;
[0029] b. Distillation of the oxidized material to recover tert-butylamine: adopt vacuum distillation method, the vacuum degree is 0.03-0.09MPa, the temperature at the top of the tower is 40-45°C, the temperature at the bottom of the tower is 50-55°C, and the distillation time is 3.5 hours;
[0030] c. The remaining material after distillation is washed with water in a centrifuge until pH = 7 to obtain the finished product of TBBS.
[0031] All the other are identical with embodiment 1.
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