Hydrogenization catalyst composition and application thereof for hydrogenization conjugated diene polyalcohol
A composition and polymer technology, applied in the direction of organic compound/hydride/coordination complex catalyst, chemical/physical process, physical/chemical process catalyst, etc. The problems of high cost and high equipment cost can achieve the effect of good activity durability, improved hydrogenation degree and low residual amount.
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Embodiment 1
[0098] After the above-mentioned preparation examples obtained the conjugated diene polymer glue, feed hydrogen (5kg / cm 2 ) to the reactor nitrogen N 2 Get rid of, and prepare the solution of each component of hydrogenation catalyst composition, dicyclopentadienyl titanium dichloride (Cp 2 TiCl 2 ) is dissolved in cyclohexane to form a 0.12% by weight solution, polymethylhydrogensiloxane is dissolved in cyclohexane to form a 0.75% by weight solution, tetrakis(isopropoxy)titanium (TPT) is dissolved in cyclohexane to form 0.2% by weight solution and n-butyllithium were dissolved in cyclohexane to form an 8% by weight solution; the prepared hydrogenation catalyst composition was added to the reactor according to the amounts in Table 1, and the hydrogenation temperature was 75 ° C. Pressure 5kg / cm 2 hydrogenation under the conditions of 8 hours to obtain the hydrogenated conjugated diene polymer of the present invention; The operating pressure and hydrogenation temperature of ...
Embodiment 2~11
[0100] The same operation mode as in Example 1, and according to the formula and hydrogenation conditions of the hydrogenation catalyst composition in Table 1, the hydrogenated conjugated diene polymer of the present invention, the degree of hydrogenation and the trans The structural residues are shown in Table 3. In addition, the hydrogenated conjugated diene polymers in Examples 2-11 have no odor, and the hydrogenated conjugated diene polymers in Examples 2-3 are yellow in appearance after thermal stability testing.
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