Ligaloes perfumes and method of producing the same
A kind of agarwood and perfume technology, which is applied to the formulation of perfume preparations, pharmaceutical formulations, cosmetic preparations, etc., to achieve the effects of simple formula, good market development prospects, and wide application range.
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Embodiment 1
[0017] Example 1. Preparation of agarwood perfume by the method of the present invention
[0018] Take 1.6Kg of agarwood raw material, pulverize it and put it into a steam distillation device, and extract it by steam distillation to obtain 4.0g extract of agarwood oil. After testing, agarwood oil mainly contains sesquiterpene components such as agarwood spiritol, α-agarwood furan, white wood acid, white wood aldehyde, and aromatic components such as benzyl acetone and p-methoxybenzyl acetone. The ingredient is the fragrance ingredient of agarwood oil.
[0019] Dissolve 4.0g agarwood oil in 95% alcohol with a weight of 100g; filter the alcohol solution to remove insoluble substances in the solution, then freeze the resulting filtrate to 5°C for 12h, and then freeze the alcohol solution After filtering, the filtrate after the second filtration is returned to room temperature to obtain agarwood perfume, which can be sold after bottling.
Embodiment 2
[0020] Example 2. Preparation of agarwood perfume by the method of the present invention
[0021] Take 708g of agarwood raw material, pulverize it and add low-boiling petroleum ether (the boiling range temperature of petroleum ether is 30~60℃) to just immerse the medicinal materials, and then use the water bath reflux method to extract, a total of 3 extractions, each extraction 1~ 3h (2h for each extraction in this example), and then the extract was decompressed in a water bath to recover the petroleum ether solvent to obtain 8.5 g of agarwood oil. After testing, agarwood oil mainly contains sesquiterpene components such as agarwood spiritol, α-agarwood furan, white wood acid, white wood aldehyde, and aromatic components such as benzyl acetone and p-methoxybenzyl acetone. The ingredient is the fragrance ingredient of agarwood oil.
[0022] Dissolve 8.5g of agarwood oil in alcohol with a concentration of 90% and a weight of 105g; filter the alcohol solution to remove insoluble subs...
Embodiment 3
[0023] Example 3. Preparation of agarwood perfume by the method of the present invention
[0024] Take 500g of agarwood raw material, pulverize it, add low-boiling petroleum ether (the boiling range temperature of petroleum ether is 30-60℃) to just immerse the medicinal materials, and then use the cold soaking method to extract, a total of 3 extractions, each extraction 5 ~ 7d, and then extract the extract in a water bath under reduced pressure to recover the organic solvent to obtain 5.5 g of agarwood oil. After testing, agarwood oil mainly contains sesquiterpene components such as agarwood spiritol, α-agarwood furan, white wood acid, white wood aldehyde, and aromatic components such as benzyl acetone and p-methoxybenzyl acetone. The ingredient is the fragrance ingredient of agarwood oil.
[0025] Dissolve 5.5g agarwood oil in 90% alcohol with a weight of 96g; filter the alcohol solution to remove insoluble substances in the solution, then freeze the filtrate to 5°C for 12 hours,...
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