Diene selection hydrogenation catalyst, and preparation method
A technology for selective hydrogenation and catalyst, which can be used in catalyst activation/preparation, hydrocarbon production by hydrogenation, catalyst support, etc., and can solve the problems of higher reaction conditions and the need for further improvement of diene hydrogenation activity, selectivity and stability. , to achieve the effect of simple preparation method, high selectivity and stability, and efficient selective hydrogenation of diene
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Embodiment 1
[0026] Put an appropriate amount of small balls with a diameter of φ1~2mm γ-Al 2 O 3 The carrier (Catalyst Plant of Fushun Petrochemical Company) was roasted in a muffle furnace at 1100°C for 4 hours. After cooling, it was used as a carrier for subsequent catalysts. 95%, the specific surface area is 101m 2 / g.
Embodiment 2
[0028] Weigh 165 grams of the alumina carrier prepared in Example 1, and use 119.3 grams of nickel nitrate Ni[(NO 3 ) 2 ·6H 2 O] and 115.5 ml of distilled water were immersed in an equal volume for 2 hours. After preliminary drying at room temperature, the catalyst A was prepared by vacuum drying at a constant temperature of 160°C for 7 hours to prepare a catalyst A with a metal Ni loading of 14.6%wt.
Embodiment 3
[0030] Put 130 grams of γ-Al balls with a diameter of φ1~2mm without high temperature treatment 2 O 3 The carrier (catalyst plant of Fushun Petrochemical Company) was prepared according to the method of Example 2 to prepare the catalyst contrast agent B with the same Ni metal content.
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