Preparation technology of ultralow contraction terylene industry long filament
A preparation process, ultra-low shrinkage technology, applied in the field of textile technology, can solve problems such as unreachable, short heating time of tow, low shrinkage rate, etc., to achieve the effect of ensuring purity and viscosity uniformity
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Embodiment 1
[0031]1. Polyethylene terephthalate (PET low-viscosity slices) undergoes solid-state polymerization to become industrial-grade high-viscosity slices that can produce industrial yarns: low-viscosity PET slices are quantitatively fed into the crystallizer through a rotary valve, and heat is circulated at 180°C. Under the action of air, it is crystallized to a crystallinity of 30%, and then fed into the roof reactor through a rotary valve with an air lock device, and undergoes solid-phase polycondensation in a nitrogen environment at 230 ° C. By adjusting the residence time and nitrogen purity, the relative viscosity A low viscosity chip of 0.67 is viscosified to a high viscosity chip of a relative viscosity of 0.9. When the high-viscosity chips are cooled to 120°C, use the nitrogen delivery system to transport the high-viscosity chips to the silo of the screw extruder.
[0032] 2. Melted and extruded by the screw extruder, sprayed out from the spinneret hole, cooled slowly, and ...
Embodiment 2
[0034] Embodiment 2, the preparation method and equipment are the same as in Example 1, except that in step 3, the first step heat setting temperature is 245°C, and the relaxation ratio is 4.4%, and the second step heat setting temperature is 240°C, and the relaxation ratio is 7.6%; The slack ratio is around 12%.
Embodiment 3
[0035] Embodiment 3, the preparation method and equipment are the same as in Example 1, except that in step 3, the first step heat setting temperature is 248°C, the relaxation ratio is 4.4%, the second step heat setting temperature is 245°C, and the relaxation ratio is 7.4%; The draw ratio is about 5.8, and the total relaxation ratio is about 11.8%.
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