Chemical modification technique for microfiltering separation film of polyvinylidene fluoride
A polyvinylidene fluoride, chemical modification technology, applied in chemical instruments and methods, semi-permeable membrane separation, membrane technology and other directions, to achieve the effects of simple operation, improved efficiency, and improved hydrophilic properties
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[0024] The specific chemical modification methods of polyvinylidene fluoride polyvinylidene fluoride hollow fiber micro-membranes and flat-plate membranes are:
[0025] 1) Preparation of polyvinylidene fluoride hollow fiber membrane and flat membrane:
[0026] Weigh a certain amount of porogen polyvinylpyrrolidone, improver polyethylene glycol and lithium chloride first dissolve with a small amount of N,N-dimethylacetamide solvent, then add to N,N-dimethylacetamide solvent Stir in;
[0027] Then weigh the polyvinylidene fluoride powder and add it into the mixed liquid, continue to stir, and heat in a water bath at the same time, and the temperature of the water bath is 85°C to 90°C. After each component is fully dissolved, control the temperature of the water bath to 40°C to 50°C, and let the casting solution stand for about 12 hours for defoaming;
[0028] The mass percentages of polyvinylidene fluoride, polyvinylpyrrolidone, polyethylene glycol, lithium chloride, and N, N-...
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