Process for extracting aluminium hydroxide from flyash
A technology of fly ash and alumina, applied in the preparation of alumina/hydroxide, alkali metal aluminate/alumina/aluminum hydroxide, etc., can solve the problems that hinder the fine development and utilization of fly ash and resource utilization problems such as low rate and low dissolution rate, to achieve the effect of high product added value, small investment and simple process
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Embodiment 1
[0024] Take 1 ton of fly ash containing 40% alumina, grind it into 300-mesh fine powder, remove iron by magnetic separation, and roast at 400°C for 1.5h to obtain activated fly ash.
[0025] Adding 72% H to activated fly ash 2 SO 4 4t, heat up to 300°C for leaching reaction for 1h, so that the alumina can be fully leached, the reacted material is separated from solid and liquid at 150°C, and the filtered residual acid is recovered and used in the next leaching process for recycling.
[0026] Add 4 t of water to the solid residue, heat up to 80°C and boil for 40 minutes, filter, wash the filter residue with water twice, and use the lotion in reverse.
[0027] The filtrate was evaporated and concentrated, and the evaporated water vapor was condensed and then returned to the stripping process. After the concentrated solution was cooled, aluminum sulfate crystals were precipitated, filtered, and 2200Kg of solid crystals were collected. The filtrate is evaporated and concentrate...
Embodiment 2
[0033] Take 1 ton of fly ash containing 40% alumina, grind it into 200-mesh fine powder, remove iron by magnetic separation, and roast at 600°C for 1 hour to obtain activated fly ash.
[0034] Add 98% H to activated fly ash 2 SO 4 2t, heat up to 250°C for 1.5h of leaching reaction, so that alumina can be fully leached, after the reaction, the material is separated from solid and liquid at 180°C, and the filtered residual acid is recovered and used in the next leaching process for recycling.
[0035] Add 6 t of water to the solid residue, raise the temperature to 75°C and boil for 45 minutes, filter, wash the filter residue twice with water, and use the lotion in reverse.
[0036] The filtrate was evaporated and concentrated, and the evaporated water vapor was condensed and then returned to the stripping process. After the concentrated solution was cooled, aluminum sulfate crystals were precipitated, filtered, and 2200Kg of solid crystals were collected. The filtrate is evap...
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