Cation emulsion asphalt anti-collapse agent for well drilling fluid and its producing method
A technology of emulsified asphalt and cations, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of restricting drilling and oil field overall benefits, collapse, irregular well diameter, etc., and reduce the occurrence of downhole complex situations, friction The effect of reducing the resistivity and suppressing collapse
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Embodiment 1
[0035] Equipment used in production: reaction kettle, metering tank, condenser, homogenizer, heat carrier heating furnace.
[0036] The production process of anti-collapse agent of the present invention is:
[0037] A. Preparation of polymer emulsion
[0038] ①Take 200kg of No. 15 industrial additive oil, add 30kg of sorbitan monooleic anhydride and mix well;
[0039] ② Add 90kg of acrylic acid monomer to 200kg of deionized water, neutralize it with 70kg of industrial grade potassium hydroxide, and prepare a monomer solution;
[0040] ③Under stirring conditions, pour the monomer solution prepared in step ② into the mixed solution in step ①, heat up to 70-80°C to form an oily emulsion, and add 1kg of dibenzoyl peroxide initiator solution dropwise , standing still after 3-4 hours of polymerization to make a polymer emulsion;
[0041] B. Preparation of cationic asphalt emulsion
[0042] ① Screen various asphalt raw materials through fluorescence analysis technology, and selec...
Embodiment 2
[0050] The production process of anti-collapse agent of the present invention is:
[0051] A. Preparation of polymer emulsion
[0052] ① Take 300kg of No. 10 industrial additive oil, add 50kg of sorbitan monooleic anhydride and mix well,
[0053] ②Add 100kg of acrylic acid monomer to 150kg of deionized water, neutralize it with 80kg of industrial grade potassium hydroxide, and prepare a monomer solution;
[0054] ③Under stirring conditions, pour the monomer solution prepared in step ② into the mixed solution in step ①, heat up to 70-80°C to form an oily emulsion, and add 2kg of dibenzoyl peroxide initiator solution dropwise , standing still after 3-4 hours of polymerization to make a polymer emulsion;
[0055] B. Preparation of cationic asphalt emulsion
[0056] ① Heat and melt 450kg of asphalt, pour it into 200kg of No. 10 industrial additive oil, add 50kg of sorbitan monooleic anhydride, stir evenly, and keep the temperature at 80-85°C;
[0057] ②Heat 300kg of deionized ...
Embodiment 3
[0063] The production process of anti-collapse agent of the present invention is:
[0064] A. Preparation of polymer emulsion
[0065] ①Take 250kg of No. 15 industrial additive oil, add 40kg of sorbitan monooleic anhydride and mix well,
[0066] ②Add 95kg of acrylic acid monomer to 180kg of deionized water, neutralize it with 75kg of industrial grade potassium hydroxide, and prepare a monomer solution;
[0067] ③Under stirring conditions, pour the monomer solution prepared in step ② into the mixed solution in step ①, heat up to 70-80°C to form an oily emulsion, and add 1.5kg of dibenzoyl peroxide initiator dropwise Solution, after 3-4 hours of polymerization reaction, stand still to make polymer emulsion;
[0068] B. Preparation of cationic asphalt emulsion
[0069] ①Heat and melt 420kg of asphalt, pour it into 200kg of No.15 industrial additive oil, add 50kg of sorbitan monooleic anhydride, stir evenly, and keep the temperature at 80-85°C;
[0070] ②Heat 200kg of deionized ...
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