Polyhydroxy binaphthalene fatty acid preparation and preparing method thereof
A technology of polyhydroxydinaphthaldehyde fatty acid and polyhydroxydinaphthaldehyde, which is applied in the field of pesticides, can solve the problems of low control level, low virus specificity, restricted control level, etc., and achieves the effects of improving safety and reducing dependence.
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[0049] Realize the process preparation method of above-mentioned polyhydroxy bis-naphthaldehyde fatty acid preparation, comprise the following steps:
[0050] 1) preparation of polyhydroxy bis-naphthaldehyde:
[0051] ① Coarsely pulverize and finely pulverize the plant tissues containing polyhydroxy bisnaphthaldehyde, such as mugwort, annua, rapeseed, mallow stalk, thimble lacquer, grass cotton root bark, euphorbia, etc., as raw material powder;
[0052] ②Weigh 500g of raw material powder and add 500ml of 75% acetone, fully stir, filter, and collect the filtrate;
[0053] ③ Add 500ml of 75% acetone to the residue, stir and filter thoroughly, and collect the filtrate;
[0054] ④ Press step ③ to repeat the extraction once;
[0055] ⑤ The filtrate mixed three times, concentrated by distillation under reduced pressure, acetone is recovered, and the steam temperature is 32°C-58°C;
[0056] ⑥ Obtain 100ml of concentrated sample, add 35ml of glacial acetic acid, and chill at -20°C...
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