Preparation for active octacosa alkanol and triaconta alkanol in rice bran

A technology of octadecanol and triacontanol, which is applied in the field of preparation of rice bran active substances octadecanol and triacontanol, and achieves the effects of improving animal physical fitness, reducing animal serum cholesterol, and achieving remarkable effects.

Inactive Publication Date: 2003-09-03
JIANGNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Domestic research on this aspect is less, and there is no report on industrialization. So far, Japan and the United States have dozens of applied patents on octacosanol, involving functional food, medicine, cosmetics and other industries, and have already occupied Considerable market share, and its industrialization also has considerable scale. On the other hand, from the current world market, octacosanol products mainly contain 10-20% products, and there are few high-purity products. A report on large-scale industrial production of octacosanol with higher purity (>50%)

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] The raw material bran wax quality index used is

[0049] Moisture: ≤0.4%

[0050] Mechanical impurity hydrate: 6.7%

[0051] Acetone soluble matter: 66.7%

[0052] Melting point (°C): 73.0, acid value: 2.7, iodine value: 52.98, saponification value: 141.2, acetone insoluble matter (%):

[0053] 33.3.

[0054] (1) Refining of bran wax, as mentioned above.

[0055] (2) For the hydrolysis of refined bran wax, the ratio of material to alkali is 1: 2, and the power of 100W is reacted for 50 minutes, and all the other conditions are the same as above.

[0056] (3) Extraction of fatty alcohol: time 10 hours, temperature 80 DEG C, solvent ratio 1: 12, all the other conditions and refining conditions of fatty alcohol are the same as above.

[0057] (4) Molecular distillation technology to separate octacosanol and triacontanol.

[0058] The octacosanol content in the mixed alcohol raw material used is 13.3%, and the triacontanol content is 25.18%. The converted molar perce...

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PUM

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Abstract

A process for prepairng octacosonal and triacontanol from rice bran, especially the rice bran wax includes such steps as refining rice bran wax, ultrasonic hydrolysis for 1 hr to extract emtrol, and molecular distilling for separating octacosanol and triacontanol. Its advantages are ultrasonic hydrolysis time decreased from 12-16 hr to 1 hr, and high purity of products (more than 80%).

Description

technical field [0001] The invention discloses a method for preparing rice bran active substances octacosanol and triacontanol, which belongs to the comprehensive utilization of rice bran, especially the comprehensive utilization of rice bran wax. Background technique [0002] Rice bran is the husk obtained by grinding the fruit body of rice, a family plant, and its content accounts for about 5-6% of rice. my country's rice output is one-third of the world's, and the annual output of rice bran reaches 9 million tons. Rice bran oil contains about 16.3%, and rice bran oil contains 3-4% wax. The potential output of rice bran wax in my country is 50,000 tons per year. Octacosanol and triacontanol are biologically active functional substances, mainly distributed in plant epidermis and germ, etc. They are abundant in rice bran wax. According to literature reports, some scholars have determined that octacosanol accounts for 12.73%. , fatty acid 1.03%. Thirty carbon fatty alcohol ...

Claims

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Application Information

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IPC IPC(8): C07C29/80C07C31/02
Inventor 王兴国刘元法
Owner JIANGNAN UNIV
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