Biodegradable lubricating grease
A biodegradable and lubricating grease technology, applied in lubricating compositions and other directions, to achieve the effect of excellent conventional physical and chemical properties
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Embodiment 1
[0020] composition:
[0021] Castor Oil: 75Wt%
[0022] Complex calcium thickener: 25Wt%
[0023] In the thickener: organic acid: calcium hydroxide = 2:1;
[0024] 12-hydroxystearic acid: octanoic acid: glacial acetic acid = 1:0.5:5
[0025] preparation:
[0026] Add molten calcium hydroxide to 1 / 2 of the base oil, add glacial acetic acid at room temperature, add n-octanoic acid when heated to about 50°C, add 12-hydroxystearic acid at around 80°C, heat up to 210°C and add remaining 1 / 2 base oil, ground three times after cooling.
Embodiment 2
[0028] composition:
[0029] Castor oil: 79.5Wt%
[0030] Composite calcium thickener: 20Wt%
[0031] Alkylated diphenylamine (SIBA Refining, L-57): 0.5wt%
[0032] In the thickener: 12-hydroxystearic acid: n-octanoic acid: glacial acetic acid = 1:0.29:5;
[0033] Organic acid: calcium hydroxide = 2:1.
[0034] Preparation: same as Example 1, just add antioxidant when cooling.
Embodiment 3
[0036] composition
[0037] Castor Oil: 89Wt%
[0038] Anhydrous calcium thickener: 11Wt%
[0039] Thickener: 12-hydroxystearic acid: calcium hydroxide = 2:1, excess calcium hydroxide 5%
[0040] preparation:
[0041] Mix 12-hydroxystearic acid and base oil, heat up to 80-85°C, add calcium hydroxide alkali solution after acid dissolution, heat up to 135°C after saponification, cool and grind three times.
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