Photomagnetic coupling type self-healing concrete as well as preparation method and device thereof
A concrete and self-healing technology, applied in clay preparation devices, cement mixing devices, chemical instruments and methods, etc., can solve the problems of uncontrollable repair of concrete, dependence on external environment changes, etc., to improve self-healing ability and enhance Brownian the effect of exercise
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0050] The technical scheme that the present invention solves the above-mentioned technical problems is as follows: a preparation method of opto-magnetic coupling type self-healing concrete, comprising the steps:
[0051] (1) Preparation of microcapsule wall material
[0052] Add urea and formaldehyde solution into the there-necked flask with a substance ratio of 1:2, after the urea is completely dissolved, adjust the pH of the solution to 8.0-9.0 with triethanolamine, and use 400-450 r / min under a constant temperature water bath at 70 °C. The mixture was stirred under reflux for 1 h to obtain a transparent and viscous urea-formaldehyde resin prepolymer.
[0053] Further, the n (urea):n (formaldehyde)=1:2 is for the purpose of generating dimethylol urea, the main component of the wall material, suppressing side reactions, and improving the productivity of effective reaction products.
[0054] (2) Preparation of magnetic core material emulsion
[0055] Weigh a certain amount ...
Embodiment 1
[0085] Example 1 Preparation of opto-magnetic coupled self-healing concrete
[0086] (1) Preparation of microcapsule wall material
[0087] Add 5 g of urea and 13.2 g of formaldehyde solution with a mass fraction of 38% into a 500 mL three-necked bottle. After all the urea is dissolved, adjust the pH of the solution to 8.0 to 9.0 with triethanolamine, and use 400 to The rotating speed of 450r / min was refluxed and stirred for 1 hour to obtain a transparent and viscous urea-formaldehyde resin prepolymer.
[0088] (2) Preparation of magnetic core material emulsion
[0089] Weigh 0.5g of black magnetic Fe 3 O 4 Nanoparticles, 0.5g composite emulsifier and 10g epoxy resin (E-51), add 200g deionized water, disperse on a high-speed dispersing homogenizer at a speed of 6000r / min for 30min to form an O / W type emulsion, the emulsification process Add 1 to 2 drops of n-octanol.
[0090] (3) Preparation of Magnetic Microcapsules
[0091] Mix the prepolymer and the core material emul...
Embodiment 2
[0095] Example 2 Performance comparison test
[0096] In the preparation method, the steps of adding magnetic materials and light guide devices are removed, and the remaining steps are the same as those in Example 1 to obtain traditional self-healing concrete; the steps of adding light guide devices are removed from the preparation method, and the remaining steps are the same as those in Example 1 to obtain magnetic self-healing concrete. Combined concrete. The traditional self-healing concrete, magnetic self-healing concrete, and opto-magnetic coupling self-healing concrete were tested for compressive strength, flexural strength, and repair rate respectively. The data obtained are shown in the following table:
[0097]
[0098] From the performance comparison data of traditional self-healing concrete, magnetic self-healing concrete and opto-magnetic coupling self-healing concrete, the analysis shows that:
[0099] a) The core material viscosity and compressive strength of...
PUM
Property | Measurement | Unit |
---|---|---|
diameter | aaaaa | aaaaa |
Tensile strength | aaaaa | aaaaa |
Tensile strength | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com